DL-Phenylalanine, N-acetyl-, 1-methylethyl ester

Base Information

• Chemical Name: DL-Phenylalanine, N-acetyl-, 1-methylethyl ester
• CAS No.: 62436-71-9
• Molecular Formula: C14H19NO3
• Molecular Weight: 249.31

Synonyms:

Chemical Property of DL-Phenylalanine, N-acetyl-, 1-methylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DL-Phenylalanine, N-acetyl-, 1-methylethyl ester

There total 2 articles about DL-Phenylalanine, N-acetyl-, 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

rac-phenylalanine isopropyl ester (18934-70-8,69655-59-0,81084-82-4) + acetic anhydride (108-24-7) → isopropyl N-acetyl-phenylalaninate (62436-71-9)

Guidance literature:

In dichloromethane; at 25 ℃; for 0.5h;

DOI:10.1021/ja907184g

Reference yield:

→ isopropyl N-acetyl-phenylalaninate (62436-71-9)

Guidance literature:

Aus entspr. Zimtsaeureester mit H2/Rh (1S,2S-3);

DOI:10.1016/0040-4020(78)89059-0

Reference yield:

isopropyl N-acetyl-phenylalaninate (62436-71-9) + methyl iodide (74-88-4) → Ac-fipe-Me

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

DOI:10.1021/ja907184g

upstream raw materials:

rac-phenylalanine isopropyl ester

acetic anhydride

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