Lithium, [(4-chlorophenyl)ethynyl]-

Base Information

Chemical Name:Lithium, [(4-chlorophenyl)ethynyl]-
CAS No.:62440-19-1
Molecular Formula:C8H4ClLi
Molecular Weight:142.514
Hs Code.:
DSSTox Substance ID:DTXSID70481160

Synonyms:Lithium, [(4-chlorophenyl)ethynyl]-;62440-19-1;SCHEMBL18245117;DTXSID70481160

Suppliers and Price of Lithium, [(4-chlorophenyl)ethynyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Lithium, [(4-chlorophenyl)ethynyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:142.0161563
Heavy Atom Count:10
Complexity:127

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[Li+].[C-]#CC1=CC=C(C=C1)Cl

Technology Process of Lithium, [(4-chlorophenyl)ethynyl]-

There total 1 articles about Lithium, [(4-chlorophenyl)ethynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873-73-4
4-n-chlorophenylacetylene

: 62440-19-1
lithium 4-chlorophenylacetylide

Guidance literature:: With n-butyllithium; In diethyl ether; at 0 ℃; for 0.25h;

Reference yield: 92.0%

: 55516-89-7
chlorotris(trimethylphosphane)cobalt(I)

: 62440-19-1
lithium 4-chlorophenylacetylide

: 594-09-2
trimethylphosphane

: (4-chlorophenyl-ethynyl)tetrakis(trimethylphosphine)cobalt

Guidance literature:: In diethyl ether; to CoCl(PMe3)4 and the acetylide condensed in vac. at -78°C is added a soln. of trimethylphosphine in ether, the mixt. is stirred at 20°C for 2 h (vac. technique, under N2); drying, the residue is extracted with pentane over a glass sinter disc, crystn. at -78°C, elem. anal.;