tetra(4-chlorophenylethynyl)tin

Base Information

• Chemical Name: tetra(4-chlorophenylethynyl)tin
• CAS No.: 2287-78-7
• Molecular Formula: C₃₂H₁₆Cl₄Sn
• Molecular Weight: 661.001

Synonyms:tetra(4-chlorophenylethynyl)tin

Chemical Property of tetra(4-chlorophenylethynyl)tin

Chemical Property:

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Technology Process of tetra(4-chlorophenylethynyl)tin

There total 3 articles about tetra(4-chlorophenylethynyl)tin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-n-chlorophenylacetylene (873-73-4) + tin(IV) chloride (7646-78-8) → tetra(4-chlorophenylethynyl)tin (2287-78-7)

Guidance literature:

With diethylamine; zinc(II) chloride; In toluene; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1039/c6nj03905g

Reference yield: 56.8%

tin(IV) chloride (7646-78-8) + lithium 4-chlorophenylacetylide (62440-19-1) → tetra(4-chlorophenylethynyl)tin (2287-78-7)

Guidance literature:

In diethyl ether; benzene; reflux for 2 h;

DOI:10.1007/BF00608040

Reference yield:

→ tetra(4-chlorophenylethynyl)tin (2287-78-7)

Guidance literature:

/BRN= 162304/, SnCl4;

DOI:10.1007/BF00608040

upstream raw materials:

tin(IV) chloride

lithium 4-chlorophenylacetylide

4-n-chlorophenylacetylene

Downstream raw materials:

1-chloro-4-[(4-nitrophenyl)ethynyl]benzene

1-(4-chlorophenyl)-3-phenylprop-2-yn-1-one

1-(4-chlorophenyl)-4-methylpent-1-yn-3-one

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