2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone

Base Information

Chemical Name:2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone
CAS No.:62459-17-0
Molecular Formula:C17H14N2OS
Molecular Weight:294.37100
Hs Code.:
Mol file:62459-17-0.mol

Synonyms:6-phenyl-2-benzylthiouracil;CCG-607;2-benzylsulfanyl-6-phenyl-3H-pyrimidin-4-one;

Suppliers and Price of 2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone

Chemical Property:

PSA：71.31000
LogP:4.14150

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone

There total 2 articles about 2-(benzylsulfanyl)-6-phenyl-4(3H)-pyrimidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 36822-11-4
2-mercapto-6-phenylpyrimidin-4(3H)-one

: 62459-17-0
2-benzylsulfanyl-6-phenyl-3H-pyrimidin-4-one

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1055/s-2002-33924

Reference yield:

: 62459-17-0
2-benzylsulfanyl-6-phenyl-3H-pyrimidin-4-one

Guidance literature:: 6-phenyl-2-thiouracil (IV), benzyl chloride, KOH, in DMF;

Reference yield: 93.0%

: 13515-76-9,116457-91-1,4465-44-5
methyl N-trityl-L-serinate

: 62459-17-0
2-benzylsulfanyl-6-phenyl-3H-pyrimidin-4-one

: 1207188-11-1
(S)-methyl 3-(2-(benzylsulfanyl)-6-phenylpyrimidin-4-yloxy)-2-(tritylamino)propanoate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.077