2,3-Dihydro-1,3-dimethyl-1H-perimidine

Base Information

Chemical Name:2,3-Dihydro-1,3-dimethyl-1H-perimidine
CAS No.:37471-00-4
Molecular Formula:C13H14N2
Molecular Weight:198.268
Hs Code.:
DSSTox Substance ID:DTXSID60190911
Wikidata:Q83063369
ChEMBL ID:CHEMBL1548816
Mol file:37471-00-4.mol

Synonyms:2,3-Dihydro-1,3-dimethyl-1H-perimidine;37471-00-4;1,3-dimethyl-2,3-dihydroperimidine;MLS000594433;SCHEMBL9161190;CHEMBL1548816;BUJSJOGOWFOHMS-UHFFFAOYSA-;DTXSID60190911;HMS2365C19;NCGC00247179-01;1,3-dimethyl-2,3-dihydro-1H-perimidine;SMR000114081;InChI=1/C13H14N2/c1-14-9-15(2)12-8-4-6-10-5-3-7-11(14)13(10)12/h3-8H,9H2,1-2H3

Suppliers and Price of 2,3-Dihydro-1,3-dimethyl-1H-perimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,3-Dihydro-1,3-dimethyl-1H-perimidine

Chemical Property:

Vapor Pressure:1.84E-05mmHg at 25°C
Boiling Point:363.1°Cat760mmHg
Flash Point:163.9°C
Density:1.134g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:198.115698455
Heavy Atom Count:15
Complexity:219

Purity/Quality:: 97-99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CN(C2=CC=CC3=C2C1=CC=C3)C

Technology Process of 2,3-Dihydro-1,3-dimethyl-1H-perimidine

There total 14 articles about 2,3-Dihydro-1,3-dimethyl-1H-perimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 20734-56-9
1,8-dimethylaminonaphthalene

: 37471-00-4
1,3-dimethyl-2,3-dihydro-1H-perimidine

Guidance literature:: In 1,4-dioxane; for 3h;
DOI:10.1021/jo00353a019

Reference yield:

: 20734-57-0
1-(N,N-dimethylamino)-8-(N-methylamino)naphthalene

: 37471-00-4
1,3-dimethyl-2,3-dihydro-1H-perimidine

Guidance literature:: Multi-step reaction with 4 steps

1: ethyl acetate / Reflux

2: hydrogen bromide / water / 1 h / 100 °C

3: ammonium hydroxide / water

4: water; dimethyl sulfoxide / 125 °C

With ammonium hydroxide; hydrogen bromide; In water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1039/c5ob01065a

Reference yield:

: 20734-58-1
N,N,N',N'-tetramethyl-1,8-diaminonaphthalene

: 37471-00-4
1,3-dimethyl-2,3-dihydro-1H-perimidine

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen bromide; potassium iodide / N,N-dimethyl-formamide / 1.5 h / Reflux

2: ethyl acetate / Reflux

3: hydrogen bromide / water / 1 h / 100 °C

4: ammonium hydroxide / water

5: water; dimethyl sulfoxide / 125 °C

With ammonium hydroxide; hydrogen bromide; potassium iodide; In water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/c5ob01065a