Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride

Base Information

Chemical Name:Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride
CAS No.:62541-62-2
Molecular Formula:C9H10INO2.ClH
Molecular Weight:327.549
Hs Code.:

Synonyms:

Suppliers and Price of Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride

There total 7 articles about Benzoic acid, 2-(2-aminoethyl)-5-iodo-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 66491-04-1
7-iodo-3,4-dihydro-1(1H)-isoquinolinone

: 62541-62-2
2-(2-Aminoethyl)-5-iodobenzoic acid hydrochloride

Guidance literature:: With hydrogenchloride; at 150 ℃; for 30h; under 31028.9 Torr;
DOI:10.1021/jo00167a015

Reference yield:

: 6552-60-9
3,4-dihydro-2H-isoquinoline-1-thione

: 62541-62-2
2-(2-Aminoethyl)-5-iodobenzoic acid hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / KOH, H₂O₂ / H₂O; methanol / 0.5 h / Ambient temperature

2: 95 percent / fuming HNO₃, conc. H₂SO₄ / 0.5 h / 0 °C

3: 93 percent / H₂ / 10percent Pd/C / methanol

4: 1) NaNO₂, 3 N HCl, 2) KI / 1) H₂O, 0 degC, 1.5 h, 2) warm to room temp., 4 h

5: 60 percent / conc. HCl / 30 h / 150 °C / 31028.9 Torr

With hydrogenchloride; potassium hydroxide; sulfuric acid; hydrogen; dihydrogen peroxide; nitric acid; potassium iodide; sodium nitrite; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo00167a015

Reference yield:

: 2257-09-2
Phenethyl isothiocyanate

: 62541-62-2
2-(2-Aminoethyl)-5-iodobenzoic acid hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 57 percent / PPA / 0.25 h / 145 °C

2: 94 percent / KOH, H₂O₂ / H₂O; methanol / 0.5 h / Ambient temperature

3: 95 percent / fuming HNO₃, conc. H₂SO₄ / 0.5 h / 0 °C

4: 93 percent / H₂ / 10percent Pd/C / methanol

5: 1) NaNO₂, 3 N HCl, 2) KI / 1) H₂O, 0 degC, 1.5 h, 2) warm to room temp., 4 h

6: 60 percent / conc. HCl / 30 h / 150 °C / 31028.9 Torr

With hydrogenchloride; potassium hydroxide; sulfuric acid; hydrogen; dihydrogen peroxide; nitric acid; potassium iodide; sodium nitrite; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo00167a015