4-Chloro-3-(chlorosulfonyl)benzoyl chloride

Base Information

Chemical Name:4-Chloro-3-(chlorosulfonyl)benzoyl chloride
CAS No.:62574-66-7
Molecular Formula:C7H3Cl3O3S
Molecular Weight:273.524
Hs Code.:
European Community (EC) Number:839-470-4
DSSTox Substance ID:DTXSID90576042
Wikidata:Q82465554

Synonyms:4-chloro-3-(chlorosulfonyl)benzoyl chloride;62574-66-7;4-chloro-3-chlorosulfonylbenzoyl chloride;SCHEMBL1926208;DTXSID90576042;PNXMCBFANZCXMB-UHFFFAOYSA-N;MFCD21090929;AKOS015954929;BS-52548;4-chloro-3-(chlorosulfonyl)benzoylchloride;E74698;EN300-279210

Suppliers and Price of 4-Chloro-3-(chlorosulfonyl)benzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
4-Chloro-3-(chlorosulfonyl)benzoyl chloride
1g
$ 432.00

Matrix Scientific
4-Chloro-3-(chlorosulfonyl)benzoyl chloride
10g
$ 1602.00

Matrix Scientific
4-Chloro-3-(chlorosulfonyl)benzoyl chloride
5g
$ 1206.00

AK Scientific
4-Chloro-3-(chlorosulfonyl)benzoylchloride
10g
$ 2212.00

AK Scientific
4-Chloro-3-(chlorosulfonyl)benzoylchloride
5g
$ 1678.00

AK Scientific
4-Chloro-3-(chlorosulfonyl)benzoylchloride
1g
$ 633.00

Total 9 raw suppliers

Chemical Property of 4-Chloro-3-(chlorosulfonyl)benzoyl chloride

Chemical Property:

Melting Point:42-43 °C(Solv: ethyl ether (60-29-7))
Boiling Point:136-138 °C(Press: 1.5 Torr)
PSA：59.59000
Density:1.663±0.06 g/cm3(Predicted)
LogP:3.72730
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:271.886848
Heavy Atom Count:14
Complexity:322

Purity/Quality:

97% ^*data from raw suppliers

4-Chloro-3-(chlorosulfonyl)benzoyl chloride ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C(=O)Cl)S(=O)(=O)Cl)Cl

Technology Process of 4-Chloro-3-(chlorosulfonyl)benzoyl chloride

There total 5 articles about 4-Chloro-3-(chlorosulfonyl)benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2494-79-3
4-chloro-3-(chlorosulfonyl)benzoic acid

: 62574-66-7
3-chlorosulfonyl-4-chlorobenzoyl chloride

Guidance literature:: With thionyl chloride; In benzene; for 8h; Heating;
DOI:10.1246/bcsj.63.2010

Reference yield:

: 5216-25-1
4-chlorotrichloromethylbenzene

: 62574-66-7
3-chlorosulfonyl-4-chlorobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfuric acid / 1) 120 deg C, 1 h 2) 150 deg C, 2 h

2: 94 percent / SOCl₂ / benzene / 8 h / Heating

With thionyl chloride; chlorosulphuric acid; In benzene;
DOI:10.1246/bcsj.63.2010

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 62574-66-7
3-chlorosulfonyl-4-chlorobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 0 - 130 °C

2: thionyl chloride / toluene / 14 h / Inert atmosphere; Reflux

With chlorosulfonic acid; thionyl chloride; In toluene;