N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine

Base Information

Chemical Name:N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine
CAS No.:62593-92-4
Molecular Formula:C14H21NSi
Molecular Weight:231.40900
Hs Code.:
DSSTox Substance ID:DTXSID20554570
Wikidata:Q82435642

Synonyms:62593-92-4;N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine;DTXSID20554570

Suppliers and Price of N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine

Chemical Property:

PSA：3.24000
LogP:3.12420
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:231.144326209
Heavy Atom Count:16
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)[Si](C)(C)C#CC1=CC=CC=C1

Technology Process of N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine

There total 4 articles about N,N-Diethyl-1,1-dimethyl-1-(phenylethynyl)silanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 6026-02-4
(N,N-diethylamino)dimethylchlorosilane

: 4440-01-1
lithium phenylacetylide

: 62593-92-4
phenylethynyl-N,N-diethylaminodimethylsilane

Guidance literature:: In tetrahydrofuran; at -78 - 25 ℃;
DOI:10.1016/S0040-4020(01)90435-1

Reference yield: 78.0%

: 6738-06-3
phenylethynylmagnesium bromide

: 6026-02-4
(N,N-diethylamino)dimethylchlorosilane

: 62593-92-4
phenylethynyl-N,N-diethylaminodimethylsilane

Guidance literature:: In diethyl ether; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1002/ejic.200900769

Reference yield:

: 6026-02-4
(N,N-diethylamino)dimethylchlorosilane

: 536-74-3
phenylacetylene

: 62593-92-4
phenylethynyl-N,N-diethylaminodimethylsilane

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

(N,N-diethylamino)dimethylchlorosilane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2020.131493