1-(1-Phenylethenyl)naphthalen-2-ol

Base Information

• Chemical Name: 1-(1-Phenylethenyl)naphthalen-2-ol
• CAS No.: 62594-99-4
• Molecular Formula: C18H14O
• Molecular Weight: 246.309
• DSSTox Substance ID: DTXSID10491384
• Nikkaji Number: J865.839K
• Wikidata: Q82335885

Synonyms:1-(1-Phenylethenyl)naphthalen-2-ol;62594-99-4;DTXSID10491384

Chemical Property of 1-(1-Phenylethenyl)naphthalen-2-ol

Chemical Property:

• Melting Point: 69-70 °C(Solv: hexane (110-54-3); ethyl ether (60-29-7))
• Boiling Point: 423.4±14.0 °C(Predicted)
• PSA: 20.23000
• Density: 1.148±0.06 g/cm3(Predicted)
• LogP: 4.60690
• XLogP3: 5.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 246.104465066
• Heavy Atom Count: 19
• Complexity: 316

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C=C(C1=CC=CC=C1)C2=C(C=CC3=CC=CC=C32)O

Technology Process of 1-(1-Phenylethenyl)naphthalen-2-ol

There total 2 articles about 1-(1-Phenylethenyl)naphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

phenylacetylene (536-74-3) + β-naphthol (135-19-3) → 1-(1-phenylethenyl)naphthalen-2-ol (62594-99-4)

Guidance literature:

With iron/aluminium-doped nanoporous KIT-5 silica (FeAl-KIT-5) catalyst; In cyclohexane; for 4h; Reflux;

DOI:10.1016/j.tetlet.2012.01.040

Reference yield: 80.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + β-naphthol (135-19-3) → 1-(1-phenylethenyl)naphthalen-2-ol (62594-99-4)

Guidance literature:

With tributyl-amine; tin(IV) chloride; In acetonitrile; for 7h; Reflux; Inert atmosphere;

DOI:10.1002/anie.201108513

Reference yield: 92.0%

trifluoromethylsulfonic anhydride (358-23-6) + 1-(1-phenylethenyl)naphthalen-2-ol (62594-99-4) → 1-(1-phenylvinyl)naphthalen-2-yl trifluoromethanesulfonate

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.202101001

upstream raw materials:

phenylacetylene

β-naphthol

styrene

Downstream raw materials:

t-butyl 1-(1-phenylethenyl)naphthalen-2-yl carbonate

1-iodomethyl-1-phenyl-1H-2,4-naphtho[2,1-d]dioxin-3-one

phenyl-1 naphto<2,1-b>furanne

C₂₄H₁₅NO₃

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