5-Phenyloxan-2-one

Base Information

Chemical Name:5-Phenyloxan-2-one
CAS No.:62618-74-0
Molecular Formula:C11H12O2
Molecular Weight:176.21200
Hs Code.:
DSSTox Substance ID:DTXSID30544982

Synonyms:5-phenyltetrahydro-2H-pyran-2-one;62618-74-0;5-Phenyloxan-2-one;tetrahydro-5-phenylpyran-2-one;SCHEMBL9336844;DTXSID30544982

Suppliers and Price of 5-Phenyloxan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
tetrahydro-5-phenylpyran-2-one 95
2g
$ 1167.00

Total 1 raw suppliers

Chemical Property of 5-Phenyloxan-2-one

Chemical Property:

PSA：26.30000
LogP:2.10720
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:176.083729621
Heavy Atom Count:13
Complexity:183

Purity/Quality:: tetrahydro-5-phenylpyran-2-one 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=O)OCC1C2=CC=CC=C2

Technology Process of 5-Phenyloxan-2-one

There total 3 articles about 5-Phenyloxan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 201230-82-2
carbon monoxide

: 6052-63-7
2-phenylbut-3-en-1-ol

: syn-3-methyl-4-phenyl-4,5-dihydrofuran-2(3H)-one

: 62618-74-0
tetrahydro-5-phenyl-2H-pyran-2-one

: anti-3-methyl-4-phenyl-4,5-dihydrofuran-2(3H)-one

Guidance literature:: carbon monoxide; 2-phenylbut-3-en-1-ol; With (acetylacetonato)dicarbonylrhodium (l); 2-isopropoxy-1-methyl-3-phenyl-2,3-dihydro-1H-benzo[d][1,3]azaphosphole; hydrogen; toluene-4-sulfonic acid; In benzene; at 45 ℃; for 16h; under 10343.2 Torr;

With sodium acetate; pyridinium chlorochromate; In dichloromethane; for 12h; Reagent/catalyst; Concentration; optical yield given as %de; regioselective reaction; Mechanism; Reactivity; Molecular sieve;
DOI:10.1021/ja803011d

Reference yield:

: 101999-42-2
(+/-)-2-phenyl-1,5-pentanediol

: 13019-37-9
α-phenyl δ-valerolactone

: 62618-74-0
tetrahydro-5-phenyl-2H-pyran-2-one

Guidance literature:: With 1-Phenylbut-1-en-3-one; dihydridotetrakis(triphenylphosphine)ruthenium; In toluene; at 20 ℃; for 10h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00361a018

Reference yield:

: 2959-96-8
2-phenylglutaric anhydride

: 13019-37-9
α-phenyl δ-valerolactone

: 62618-74-0
tetrahydro-5-phenyl-2H-pyran-2-one

Guidance literature:: With sodium tetrahydroborate; In N,N-dimethyl-formamide; for 1.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;