5-Hydroxy-2,3-dimethoxybenzaldehyde

Base Information

Chemical Name:5-Hydroxy-2,3-dimethoxybenzaldehyde
CAS No.:62648-55-9
Molecular Formula:C9H10O4
Molecular Weight:182.176
Hs Code.:
DSSTox Substance ID:DTXSID40576991
Wikidata:Q82466893

Synonyms:5-hydroxy-2,3-dimethoxybenzaldehyde;62648-55-9;DTXSID40576991

Suppliers and Price of 5-Hydroxy-2,3-dimethoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Hydroxy-2,3-dimethoxybenzaldehyde

Chemical Property:

PSA：55.76000
LogP:1.22190
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:182.05790880
Heavy Atom Count:13
Complexity:171

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1OC)C=O)O

Technology Process of 5-Hydroxy-2,3-dimethoxybenzaldehyde

There total 4 articles about 5-Hydroxy-2,3-dimethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6324-49-8
2,3-dimethoxy-5-nitrobenzaldehyde

: 62648-55-9
5-hydroxy-2,3-dimethoxybenzaldehyde

Guidance literature:: With sodium hydrogensulfite; iron(II) sulfate; calcium carbonate; Reagens 4:Wasser;Behandeln der filtrierten Reaktionsloesung mit wss.HCl und mit wss.NaNO₂ bei 3grad und Erwaermen der erhaltenen Diazoniumsalz-Loesung;
DOI:10.1021/ja01359a033

Reference yield:

: 93092-14-9
1-bromo-5-hydroxy-2,3-dimethoxybenzene

: 62648-55-9
5-hydroxy-2,3-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide

2: Raney-Ni, 70percent HCOOH / 4 h / Heating

With formic acid; nickel; In N,N-dimethyl-formamide;