1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER

Base Information

Chemical Name:1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER
CAS No.:62677-71-8
Molecular Formula:C14H16O2
Molecular Weight:216.28
Hs Code.:
Mol file:62677-71-8.mol

Synonyms:

Suppliers and Price of 1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER 95.00%
5MG
$ 497.13

Total 6 raw suppliers

Chemical Property of 1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER

Chemical Property:

Vapor Pressure:8.94E-05mmHg at 25°C
Boiling Point:339.9oC at 760 mmHg
Flash Point:202.1oC
PSA：26.30000
Density:1.138g/cm3
LogP:2.96940

Purity/Quality:

97% ^*data from raw suppliers

1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER

There total 5 articles about 1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLIDINE ACETATIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 62677-71-8
4-(carbethoxymethylene)-1,2,3,4-tetrahydronaphthalene

: 54125-45-0
2-(3,4-dihydro-naphthalen-1-yl)-acetic acid ethyl ester

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h; Inert atmosphere;

3,4-dihydronaphthalene-1(2H)-one; In tetrahydrofuran; for 16h; Inert atmosphere; Reflux;

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 62677-71-8
4-(carbethoxymethylene)-1,2,3,4-tetrahydronaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / zinc, iodine / tetrahydrofuran / 3.5 h / Heating

2: P₂O₅ / benzene / 2 h / Heating

With iodine; phosphorus pentoxide; zinc; In tetrahydrofuran; benzene;
DOI:10.1021/ja00267a036

Reference yield:

: 91111-41-0
α,α'-Hydroxytrihydronaphthylessigsaeureethylester

: 62677-71-8
4-(carbethoxymethylene)-1,2,3,4-tetrahydronaphthalene

: 54125-45-0
2-(3,4-dihydro-naphthalen-1-yl)-acetic acid ethyl ester

Guidance literature:: With phosphorus pentoxide; In benzene; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1021/ja00267a036