Propanoic acid, 2-[(2,4-dinitrophenyl)hydrazono]-, methyl ester, (Z)-

Base Information

• Chemical Name: Propanoic acid, 2-[(2,4-dinitrophenyl)hydrazono]-, methyl ester, (Z)-
• CAS No.: 62740-61-8
• Molecular Formula: C₁₀H₁₀N₄O₆
• Molecular Weight: 282.213

Synonyms:2-((Z)-2,4-dinitro-phenylhydrazono)-propionic acid methyl ester;Brenztraubensaeuremethylester-2,4-dinitrophenylhydrazon;Propanoic acid,2-[(2,4-dinitrophenyl)hydrazono]-,methyl ester,(E);2-((Z)-2,4-Dinitro-phenylhydrazono)-propionsaeure-methylester;Propanoic acid,2-[(2,4-dinitrophenyl)hydrazono]-,methyl ester,(Z);

Chemical Property of Propanoic acid, 2-[(2,4-dinitrophenyl)hydrazono]-, methyl ester, (Z)-

Chemical Property:

• PSA: 142.33000
• LogP: 2.58320

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Propanoic acid, 2-[(2,4-dinitrophenyl)hydrazono]-, methyl ester, (Z)-

There total 4 articles about Propanoic acid, 2-[(2,4-dinitrophenyl)hydrazono]-, methyl ester, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) → 2-((Z)-2,4-dinitro-phenylhydrazono)-propionic acid methyl ester (62740-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / methanol

2: HCl / 1.5 h / 85 °C

With hydrogenchloride; In methanol;

DOI:10.1271/bbb.60264

Reference yield:

2-(2,4-dinitrophenylhydrazono)-propanoic acid (790-12-5) → 2-((Z)-2,4-dinitro-phenylhydrazono)-propionic acid methyl ester (62740-61-8)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂

With thionyl chloride;

Reference yield:

Methyl-N-benzyloxy-2-methylmaleamat (56439-43-1) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 2-((Z)-2,4-dinitro-phenylhydrazono)-propionic acid methyl ester (62740-61-8)

Guidance literature:

Multistep reaction; (i) O₃, (ii) /BRN= 615586/, H₂SO₄;

DOI:10.1039/P19750000825

upstream raw materials:

methanol

2-(2,4-dinitro-phenylhydrazono)-propionyl chloride

Methyl-N-benzyloxy-2-methylmaleamat

(2,4-dinitro-phenyl)-hydrazine

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