Technology Process of Benzenemethanamine, N-[1-(1-methylethyl)pentyl]-
There total 3 articles about Benzenemethanamine, N-[1-(1-methylethyl)pentyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen;
In
Isopropyl acetate;
at 24 ℃;
for 24h;
under 11251.1 Torr;
DOI:10.1002/adsc.201100250
- Guidance literature:
-
isobutylidenebenzylamine;
With
titanium(IV) isopropylate; n-butyllithium;
In
diethyl ether; hexane;
at -78 - 20 ℃;
for 1h;
Inert atmosphere;
2-methyl-3-buten-2-ol;
With
n-butyllithium;
In
tetrahydrofuran; diethyl ether; hexane;
at -78 - 20 ℃;
for 12h;
Inert atmosphere;
With
water; ammonium chloride;
In
tetrahydrofuran; diethyl ether; hexane;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol901870n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: titanium(IV) isopropylate / Isopropyl acetate / 0.5 h
2: 5%-palladium/activated carbon; hydrogen / Isopropyl acetate / 24 h / 24 °C / 11251.1 Torr
With
titanium(IV) isopropylate; 5%-palladium/activated carbon; hydrogen;
In
Isopropyl acetate;
DOI:10.1002/adsc.201100250