4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane
CAS No.:627526-54-9
Molecular Formula:C₁₆H₂₃BO₂
Molecular Weight:258.168
Hs Code.:2934999090
Mol file:627526-54-9.mol

Synonyms:

Suppliers and Price of 4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane 95+%
5g
$ 847.00

Chemenu
4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane 98%
1g
$ 229.00

Alichem
4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane
5g
$ 940.50

AK Scientific
5,6,7,8-Tetrahydronaphthalene-2-boronicacidpinacolester
5g
$ 1207.00

Total 10 raw suppliers

Chemical Property of 4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Chemical Property:

Boiling Point:365.6±31.0 °C(Predicted)
PSA：18.46000
Density:1.02±0.1 g/cm3(Predicted)
LogP:2.86460
Storage Temp.:Room temperature.

Purity/Quality:

97% ^*data from raw suppliers

4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

There total 15 articles about 4,4,5,5-Tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 119-64-2
tetralin

: 13517-10-7
boron triiodide

: 627526-54-9
4,4,5,5-tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Guidance literature:: tetralin; boron triiodide; In neat (no solvent); at 220 ℃; for 12h;

2,3-dimethyl-2,3-butane diol; With triethylamine; at 20 ℃; for 0.5h;

Reference yield: 81.0%

: (E)-1-(5,6,7,8-tetrahydronaphthalen-2-yl)ethan-1-one O-perfluorobenzoyl oxime

: 73183-34-3
bis(pinacol)diborane

: 627526-54-9
4,4,5,5-tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Guidance literature:: With 2,6-di-tert-butyl-4-methyl-phenol; potassium carbonate; 2-(4,5-dihydro-4,4-dimethyl-2-oxazolyl)pyridine; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; tris<3,5-bis(trifluoromethyl)phenyl>phosphane; palladium dichloride; In 1,2-dichloro-ethane; at 120 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.202006740

Reference yield: 79.0%

: tert-butyldimethyl((5,6,7,8-tetrahydronaphthalen-2-yl)oxy)silane

: 73183-34-3
bis(pinacol)diborane

: 627526-54-9
4,4,5,5-tetramethyl-2-(5,6,7,8-tetrahydronaphthalen-2-yl)-1,3,2-dioxaborolane

Guidance literature:: With bis(acetylacetonate)nickel(II); lithium tert-butoxide; at 100 ℃; for 16h; Sealed tube;
DOI:10.1021/acs.orglett.1c01280