Tert-butyl 3,4-diaminobenzoate

Base Information

Chemical Name:Tert-butyl 3,4-diaminobenzoate
CAS No.:62754-26-1
Molecular Formula:C11H16N2O2
Molecular Weight:208.26
Hs Code.:
European Community (EC) Number:827-948-5
DSSTox Substance ID:DTXSID50565033
Wikidata:Q82449951

Synonyms:tert-butyl 3,4-diaminobenzoate;62754-26-1;Benzoic acid, 3,4-diamino-, 1,1-dimethylethyl ester;tert-butyl3,4-diaminobenzoate;SCHEMBL11090176;DTXSID50565033;MFCD20039955;SB78146;3,4-diamino-benzoic acid tert-butyl ester;CS-0253361;EN300-640690

Suppliers and Price of Tert-butyl 3,4-diaminobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Tert-butyl 3,4-diaminobenzoate

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:208.121177757
Heavy Atom Count:15
Complexity:235

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)C1=CC(=C(C=C1)N)N

Technology Process of Tert-butyl 3,4-diaminobenzoate

There total 3 articles about Tert-butyl 3,4-diaminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62754-22-7
tert-butyl 3,4-dinitrobenzoate

: 62754-26-1
tert-butyl 3,4-diaminobenzoate

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 90 ℃; for 2h;

Reference yield:

concentrated H₂ SO₄: concentrated H₂ SO₄

: 115-11-7,15220-85-6
isobutene

: 619-05-6
3,4-diaminobenzoic acid

: 62754-26-1
tert-butyl 3,4-diaminobenzoate

Guidance literature:: In 1,4-dioxane; water;

Reference yield:

: 528-45-0
3,4-dinitrobenzoic acid

: 62754-26-1
tert-butyl 3,4-diaminobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 16 h / 0 - 20 °C / Inert atmosphere

2: iron; ammonium chloride / ethanol; water / 2 h / 90 °C

With dmap; iron; ammonium chloride; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;