Furo[3,4-f]-1,3-benzodioxol-5(7H)-one, 7-hydroxy-

Base Information

• Chemical Name: Furo[3,4-f]-1,3-benzodioxol-5(7H)-one, 7-hydroxy-
• CAS No.: 62869-57-2
• Molecular Formula: C9H6O5
• Molecular Weight: 194.14100
• Mol file: 62869-57-2.mol

Synonyms:7-hydroxy-7H-furo[3',4':4,5]benzo[1,2-d][1,3]dioxol-5-one;Furo[3,4-f]-1,3-benzodioxol-5(7H)-one,7-hydroxy;7-hydroxyfuro[3,4-f][1,3]benzodioxol-5(7H)-one;5,6-(methylenedioxy)phthalaldehydic acid;3-Hydroxy-5,6-dioxymethylenphthalid;

Chemical Property of Furo[3,4-f]-1,3-benzodioxol-5(7H)-one, 7-hydroxy-

Chemical Property:

• Melting Point: 165-167 °C
• Boiling Point: 461.8±45.0 °C(Predicted)
• PSA: 64.99000
• Density: 1.699±0.06 g/cm3(Predicted)
• LogP: 0.57660

Purity/Quality:

12-hydroxy-4,6,11-trioxatricyclo[7.3.0.0,3,7]dodeca-1,3(7),8-trien-10-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Furo[3,4-f]-1,3-benzodioxol-5(7H)-one, 7-hydroxy-

There total 2 articles about Furo[3,4-f]-1,3-benzodioxol-5(7H)-one, 7-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon dioxide (124-38-9,18923-20-1) + 6-bromo-3,4-methylenedioxybenzaldehyde (15930-53-7) → 5,6-(methylenedioxy)phthalaldehydic acid (62869-57-2)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jo00162a011

Reference yield:

→ 5,6-(methylenedioxy)phthalaldehydic acid (62869-57-2)

Guidance literature:

5,6-Dioxymethylenphthalid, NBS/Benzoylperoxid/H2O;

Reference yield: 44.0%

5,6-(methylenedioxy)phthalaldehydic acid (62869-57-2) → 4,5-methylendioxyphtalaldehydic acid (51877-66-8)

Guidance literature:

With potassium carbonate; In water; at 80 ℃;

upstream raw materials:

carbon dioxide

6-bromo-3,4-methylenedioxybenzaldehyde

Downstream raw materials:

4,5-methylendioxyphtalaldehydic acid