Tetradecanoic acid, (2R,14R)-5,11-bis(2-chlorophenoxy)-5,11-dioxido-8-(phenylmethoxy)-4, 6,10,12-tetraoxa-5,11-diphosphapentadecane-1,2,14,15-tetrayl ester

Base Information

• Chemical Name: Tetradecanoic acid, (2R,14R)-5,11-bis(2-chlorophenoxy)-5,11-dioxido-8-(phenylmethoxy)-4, 6,10,12-tetraoxa-5,11-diphosphapentadecane-1,2,14,15-tetrayl ester
• CAS No.: 628722-33-8
• Molecular Formula: C84H138Cl2O17P2
• Molecular Weight: 1552.86

Synonyms:

Chemical Property of Tetradecanoic acid, (2R,14R)-5,11-bis(2-chlorophenoxy)-5,11-dioxido-8-(phenylmethoxy)-4, 6,10,12-tetraoxa-5,11-diphosphapentadecane-1,2,14,15-tetrayl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tetradecanoic acid, (2R,14R)-5,11-bis(2-chlorophenoxy)-5,11-dioxido-8-(phenylmethoxy)-4, 6,10,12-tetraoxa-5,11-diphosphapentadecane-1,2,14,15-tetrayl ester

There total 2 articles about Tetradecanoic acid, (2R,14R)-5,11-bis(2-chlorophenoxy)-5,11-dioxido-8-(phenylmethoxy)-4, 6,10,12-tetraoxa-5,11-diphosphapentadecane-1,2,14,15-tetrayl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1,2-dimyristoyl-sn-glycerol (60562-16-5,56270-93-0) + 2-O-benzylglycerol (14690-00-7) + 2-chlorophenyl dichlorophosphate (15074-54-1) → Tetradecanoic acid (R)-2-[{2-benzyloxy-3-[((R)-2,3-bis-tetradecanoyloxy-propoxy)-(2-chloro-phenoxy)-phosphoryloxy]-propoxy}-(2-chloro-phenoxy)-phosphoryloxy]-1-tetradecanoyloxymethyl-ethyl ester (628722-33-8)

Guidance literature:

1,2-dimyristoyl-sn-glycerol; 2-chlorophenyl dichlorophosphate; With pyridine; In dichloromethane; at 0 - 20 ℃; for 2.75h;

2-O-benzylglycerol; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 72.0%

2-O-benzylglycerol (14690-00-7) + Tetradecanoic acid (R)-2-[chloro-(2-chloro-phenoxy)-phosphoryloxy]-1-tetradecanoyloxymethyl-ethyl ester → Tetradecanoic acid (R)-2-[{2-benzyloxy-3-[((R)-2,3-bis-tetradecanoyloxy-propoxy)-(2-chloro-phenoxy)-phosphoryloxy]-propoxy}-(2-chloro-phenoxy)-phosphoryloxy]-1-tetradecanoyloxymethyl-ethyl ester (628722-33-8)

Guidance literature:

In dichloromethane; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2004.07.084

Reference yield: 87.0%

Tetradecanoic acid (R)-2-[{2-benzyloxy-3-[((R)-2,3-bis-tetradecanoyloxy-propoxy)-(2-chloro-phenoxy)-phosphoryloxy]-propoxy}-(2-chloro-phenoxy)-phosphoryloxy]-1-tetradecanoyloxymethyl-ethyl ester (628722-33-8) → 2-O-benzyl-1,3-bis(1,2-O-dimyristoyl-sn-glycero-3-phosphoryl)glycerol diammonium salt

Guidance literature:

With 2-pyridinealdoxime; water; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; at 20 ℃; for 2.5h;

upstream raw materials:

2-O-benzylglycerol

1,2-dimyristoyl-sn-glycerol

2-chlorophenyl dichlorophosphate

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