1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene

Base Information

Chemical Name:1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene
CAS No.:62907-50-0
Molecular Formula:C19H18
Molecular Weight:246.352
Hs Code.:
DSSTox Substance ID:DTXSID90503393

Synonyms:62907-50-0;DTXSID90503393;1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene;3-allyl-3-methyl-1,2-diphenylcyclopropene

Suppliers and Price of 1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:246.140850574
Heavy Atom Count:19
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=C1C2=CC=CC=C2)C3=CC=CC=C3)CC=C

Technology Process of 1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene

There total 8 articles about 1,1'-[3-Methyl-3-(prop-2-en-1-yl)cycloprop-1-ene-1,2-diyl]dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 73377-62-5
(E)-1,2-diphenyl-3-hydroxy-3-methyl-1,5-hexadiene

: 74-88-4
methyl iodide

: 73377-56-7
(E)-3-methyl-3-methoxy-1,2-diphenyl-1,5-hexadiene

: 62907-50-0
1,2-diphenyl-3-allyl-3-methylcyclopropene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/jo01299a029

Reference yield: 31.0%

: 72612-89-6,75032-50-7,84537-34-8
3-methyl-1,2-diphenylcyclopropenylium perchlorate

: 1730-25-2
allylmagnesium bromide

: 62907-50-0
1,2-diphenyl-3-allyl-3-methylcyclopropene

: 62907-51-1
1,3-diphenyl-2-methyl-3-allylcyclopropene

Guidance literature:: In diethyl ether; at -78 ℃; for 4h;
DOI:10.1021/ja00528a047

Reference yield:

: 72612-89-6,75032-50-7,84537-34-8
3-methyl-1,2-diphenylcyclopropenylium perchlorate

: 62907-50-0
1,2-diphenyl-3-allyl-3-methylcyclopropene

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / diethyl ether / 4 h / -78 °C

2: 35 percent Spectr_. / pyridine; benzene / thermolysis

In pyridine; diethyl ether; benzene;
DOI:10.1021/ja00528a047