Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Base Information

Chemical Name:Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate
CAS No.:123044-11-1
Molecular Formula:C₁₆H₁₈N₂O₃S
Molecular Weight:318.397
Hs Code.:
DSSTox Substance ID:DTXSID70924360
Mol file:123044-11-1.mol

Synonyms:DTXSID70924360;123044-11-1;Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Suppliers and Price of Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Chemical Property:

Vapor Pressure:1.62E-07mmHg at 25°C
Boiling Point:427.6°Cat760mmHg
Flash Point:212.4°C
Density:1.28g/cm³
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:318.10381361
Heavy Atom Count:22
Complexity:498

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(N(C(=S)N(C1C2=CC=CC=C2)C=O)C)C
Isomeric SMILES:CCOC(=O)C1=C(N(C(=S)N([C@H]1C2=CC=CC=C2)C=O)C)C

Technology Process of Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate

There total 3 articles about Ethyl 3-formyl-1,6-dimethyl-4-phenyl-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141-97-9
ethyl acetoacetate

: 123044-11-1
1,6-dimethyl-3-formyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / conc HCl / ethanol / 3 h / Heating

2: 1.) phosphorus oxychloride, 2.) H₂O / 1.) room temperature, 15 min

With hydrogenchloride; water; trichlorophosphate; In ethanol;

Reference yield:

: 100-52-7
benzaldehyde

: 123044-11-1
1,6-dimethyl-3-formyl-4-phenyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / conc HCl / ethanol / 3 h / Heating

2: 1.) phosphorus oxychloride, 2.) H₂O / 1.) room temperature, 15 min

With hydrogenchloride; water; trichlorophosphate; In ethanol;