5-Isosylveterpinolene

Base Information

Chemical Name:5-Isosylveterpinolene
CAS No.:25946-29-6
Molecular Formula:C10H16
Molecular Weight:136.237
Hs Code.:
DSSTox Substance ID:DTXSID301267218
Nikkaji Number:J1.065.298G
Metabolomics Workbench ID:45939
Mol file:25946-29-6.mol

Synonyms:5-Isosylveterpinolene;1-Methyl-5-(1-methylethylidene)cyclohexene;Isosylveterpinolene;WPOQYXKDKVBMSB-UHFFFAOYSA-N;DTXSID301267218;1-methyl-5-(propan-2-ylidene)cyclohex-1-ene;25946-29-6

Suppliers and Price of 5-Isosylveterpinolene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 5-Isosylveterpinolene

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:136.125200510
Heavy Atom Count:10
Complexity:178

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCCC(=C(C)C)C1

Technology Process of 5-Isosylveterpinolene

There total 4 articles about 5-Isosylveterpinolene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 107-86-8
3,3-dimethyl acrylaldehyde

: 78-79-5,9003-31-0
isoprene

: 586-62-9,69073-38-7
Terpinolene

: 25946-29-6
isosylveterpinolene

Guidance literature:: formaldehyd; 3,3-dimethyl acrylaldehyde; isoprene; With pyrrolidine; propionic acid; In water; at 100 ℃; for 16h; Autoclave;

In toluene; at 450 ℃; Inert atmosphere; quartz tube; Gas phase;
DOI:10.1002/chem.200800145

Reference yield:

: 1193-18-6
3-methylcyclohexen-2-one

: 25946-29-6
isosylveterpinolene

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / adipic acid / 4 h / 213 °C / distillation

2: 1.) BuLi, (iPr)2NH / 1.) hexane/THF, 50 deg C, 2 h, 2.) THF/hexane, -40 deg C, 2 h

3: 71 percent / dimethylformamide dimethyl acetal / CH₂Cl₂ / 1.) 2 h, reflux, 2.) 14 h, RT

With n-butyllithium; Adipic acid; N,N-dimethyl-formamide dimethyl acetal; diisopropylamine; In dichloromethane;
DOI:10.1002/(SICI)1522-2675(19990113)82:1<53::AID-HLCA53>3.0.CO;2-7

Reference yield:

: 31883-98-4
3-methylcyclohex-3-en-1-one

: 25946-29-6
isosylveterpinolene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi, (iPr)2NH / 1.) hexane/THF, 50 deg C, 2 h, 2.) THF/hexane, -40 deg C, 2 h

2: 71 percent / dimethylformamide dimethyl acetal / CH₂Cl₂ / 1.) 2 h, reflux, 2.) 14 h, RT

With n-butyllithium; N,N-dimethyl-formamide dimethyl acetal; diisopropylamine; In dichloromethane;
DOI:10.1002/(SICI)1522-2675(19990113)82:1<53::AID-HLCA53>3.0.CO;2-7