Carbamic acid, 4-piperidinyl-,(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

Base Information

• Chemical Name: Carbamic acid, 4-piperidinyl-,(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester
• CAS No.: 629957-82-0
• Molecular Formula: C29H33F7N4O3
• Molecular Weight: 618.595

Synonyms:

Chemical Property of Carbamic acid, 4-piperidinyl-,(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

Chemical Property:

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Technology Process of Carbamic acid, 4-piperidinyl-,(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

There total 1 articles about Carbamic acid, 4-piperidinyl-,(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-4-(1-benzylpiperidine-4-yl)aminocarbonyloxy-2-(4-fluoro-2-methylphenyl)piperidine → (2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-(4-piperidinyl)aminocarbonyloxypiperidine (629957-82-0)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 4.5h;

Reference yield:

(2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-(4-piperidinyl)aminocarbonyloxypiperidine (629957-82-0) + 3-Hydroxy-3-methylbutyric acid (625-08-1) → (2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-{1-(3-hydroxy-3-methylbutyryl)piperidine-4-yl}aminocarbonyloxypiperidine (629948-76-1)

Guidance literature:

With 1,1'-carbonyldiimidazole; In dichloromethane; at 20 ℃;

Reference yield:

(2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-(4-piperidinyl)aminocarbonyloxypiperidine (629957-82-0) → C33H39F7N4O5 (629948-83-0)

Guidance literature:

Downstream raw materials:

(2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-{1-(3-hydroxy-3-methylbutyryl)piperidine-4-yl}aminocarbonyloxypiperidine

C₃₃H₃₉F₇N₄O₅

C₃₃H₃₉F₇N₄O₅

C₃₃H₃₉F₇N₄O₅

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