Cyclopropanecarboxylic acid, 1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6 H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]-

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6 H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]-
CAS No.:630382-45-5
Molecular Formula:C24H20F3N3O4
Molecular Weight:471.436
Hs Code.:

Cyclopropanecarboxylic acid,
1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6
H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]-

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Chemical Property of Cyclopropanecarboxylic acid, 1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6 H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]-

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Technology Process of Cyclopropanecarboxylic acid, 1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6 H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]-

There total 1 articles about Cyclopropanecarboxylic acid, 1-[4-[1,4,5,7-tetrahydro-1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-6 H-pyrazolo[3,4-c]pyridin-6-yl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 124276-89-7
1-(4-iodophenyl)cyclopropane-1-carboxylic acid

: 630382-44-4
1-(4-methoxyphenyl)-3-(trifluoromethyl)-5,6-dihydro-1H-pyrazolo[3,4-c]pyridin-7(4H)-one

: 630382-45-5
1-{4-[1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}cyclopropanecarboxylic acid

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In dimethyl sulfoxide; at 130 ℃; for 24h;
DOI:10.1016/j.bmcl.2008.05.095

Reference yield: 95.0%

: 630382-45-5
1-{4-[1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}cyclopropanecarboxylic acid

: 630382-46-6
6-{4-[1-(hydroxymethyl) cyclopropyl] phenyl}-l-(4-methoxyphenyl)-3-(trifluoromethyl)-1,4,5,6-tetrahydro-7H-pyrazolo[3,4-c]pyridin-7-one

Guidance literature:: 1-{4-[1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}cyclopropanecarboxylic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 ℃; for 0.333333h;
DOI:10.1016/j.bmcl.2008.05.095

Reference yield: 67.0%

: 123-75-1
pyrrolidine

: 630382-45-5
1-{4-[1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}cyclopropanecarboxylic acid

: 1-(4-methoxyphenyl)-6-(4-[1-(1-pyrrolidinylcarbonyl)cyclopropyl] phenyl)-3-(trifluoromethyl)-1,4,5,6-tetrahydro-7H-pyrazolo[3,4-c]pyridin-7-one

Guidance literature:: 1-{4-[1-(4-methoxyphenyl)-7-oxo-3-(trifluoromethyl)-1,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridin-6-yl]phenyl}cyclopropanecarboxylic acid; With thionyl chloride; In dichloromethane; at 20 ℃; for 1h;

pyrrolidine; With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;