6,7-Dimethoxynaphthalene-2-sulfonyl chloride

Base Information

Chemical Name:6,7-Dimethoxynaphthalene-2-sulfonyl chloride
CAS No.:63093-17-4
Molecular Formula:C₁₂H₁₁ClO₄S
Molecular Weight:286.736
Hs Code.:
DSSTox Substance ID:DTXSID00560578
Wikidata:Q82443997

Synonyms:6,7-dimethoxynaphthalene-2-sulfonyl chloride;63093-17-4;SCHEMBL2328500;DTXSID00560578;WTUCGFYIXJREBR-UHFFFAOYSA-N;AKOS015934967;6,7-dimethoxy-2-naphthalenesulfonyl chloride;6.7-dimethoxy-2-naphthalenesulfonyl chloride

Suppliers and Price of 6,7-Dimethoxynaphthalene-2-sulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6,7-Dimethoxynaphthalene-2-sulfonyl chloride

Chemical Property:

PSA：60.98000
LogP:3.86530
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:286.0066577
Heavy Atom Count:18
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C2C=C(C=CC2=C1)S(=O)(=O)Cl)OC

Technology Process of 6,7-Dimethoxynaphthalene-2-sulfonyl chloride

There total 1 articles about 6,7-Dimethoxynaphthalene-2-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67434-28-0
2-isocyano-1-(piperidin-1-yl) ethan-1-one

: 63093-17-4
2-(6,7-Dimethoxynaphthalenyl)sulfonyl chloride

Guidance literature:

Reference yield: 66.0%

: 63093-17-4
2-(6,7-Dimethoxynaphthalenyl)sulfonyl chloride

: 63093-18-5
4-(L-arginyl)-morpholine

: 4-[N2-(6,7-dimethoxy-2-naphthalenesulfonyl)-L-arginyl]morpholine acetate

Guidance literature:: With acetic acid; triethylamine; In chloroform; water;

Reference yield:

: 63093-17-4
2-(6,7-Dimethoxynaphthalenyl)sulfonyl chloride

: 66937-16-4
N₂-(6,7-dimethoxy-2-naphthalenesulfonyl)-L-arginyl-N-cyclohexylglycine

Guidance literature:: Multi-step reaction with 4 steps

1: 71.6 percent / K₂CO₃ / H₂O; benzene / 3 h / 60 °C

2: SOCl₂, DMF / 4 h / Ambient temperature

3: Et₃N / CHCl₃ / 3 h / Ambient temperature

4: HCl / CHCl₃; ethyl acetate / 5 h / Ambient temperature

With hydrogenchloride; thionyl chloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In chloroform; water; ethyl acetate; benzene;
DOI:10.1021/jm00186a003