4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline

Base Information

• Chemical Name: 4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline
• CAS No.: 63212-69-1
• Molecular Formula: C15H17NOTe
• Molecular Weight: 354.906
• DSSTox Substance ID: DTXSID40506930
• Nikkaji Number: J485.092K
• Wikidata: Q82362908
• Mol file: 63212-69-1.mol

Synonyms:63212-69-1;4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline;SCHEMBL11145489;DTXSID40506930

Chemical Property of 4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 357.0372369
• Heavy Atom Count: 18
• Complexity: 231

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)[Te]C2=CC=C(C=C2)OC

Technology Process of 4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline

There total 6 articles about 4-[(4-Methoxyphenyl)tellanyl]-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-(p-methoxyphenyl)tellurium oxide (57857-70-2) + bis telluroxide (65683-57-0) → bis [4-(N,N-dimethylamino)phenyl] telluride (59130-74-4) + p-dimethylaminophenyl(p-methoxyphenyl)tellurium(II) (63212-69-1) + (4-methoxyphenoxy)tri(4-methoxyphenyl)tellurane + (4-dimethylaminophenoxy)tri(4-dimethylaminophenyl)tellurane + (4-dimethylaminophenoxy)di(4-methoxyphenyl)(4-dimethylaminophenyl)tellurane + (4-methoxyphenoxy)di-(4-dimethylaminophenyl)(4-methoxyphenyl)tellurane + p-(dimethylamino)phenyl p-methoxyphenyl telluroxide (80246-39-5) + N,N-dimethyl-aniline (121-69-7,77733-26-7)

Guidance literature:

In toluene; for 4h; Reflux;

DOI:10.1007/s11172-017-1784-x

Reference yield:

tellurium dichloride (63971-78-8) → p-dimethylaminophenyl(p-methoxyphenyl)tellurium(II) (63212-69-1)

Guidance literature:

With sodium sulfide;

DOI:10.1016/0040-4020(61)80037-9

Reference yield:

p-methoxyphenyltellurium trichloride (36309-68-9) → p-dimethylaminophenyl(p-methoxyphenyl)tellurium(II) (63212-69-1)

Guidance literature:

Multi-step reaction with 2 steps

2: Na₂S

With sodium sulfide;

DOI:10.1016/0040-4020(61)80037-9

upstream raw materials:

tellurium dichloride

<4-Methoxy-phenyl>-<4-dimethylamino-phenyl>-tellurdibromid

p-methoxyphenyltellurium trichloride

p-methoxyphenyltellurium tribromide

Downstream raw materials:

cholesteryl benzoate

<4-Methoxy-phenyl>-<4-dimethylamino-phenyl>-tellurdiiodid

<4-Methoxy-phenyl>-<4-dimethylamino-phenyl>-tellurdibromid