Benzoic acid, 4-azido-, hydrazide

Base Information

• Chemical Name: Benzoic acid, 4-azido-, hydrazide
• CAS No.: 63296-32-2
• Molecular Formula: C₇H₇N₅O
• Molecular Weight: 177.165
• Hs Code.: 2928009090
• European Community (EC) Number: 809-975-4
• DSSTox Substance ID: DTXSID70431029
• Wikidata: Q82244815
• Mol file: 63296-32-2.mol

Synonyms:4-azidobenzohydrazide;63296-32-2;p-Azidobenzoylhydrazide;Benzoic acid, 4-azido-, hydrazide;4-AZIDOBENZOYL HYDRAZINE;4-Azidobenzoic acid hydrazide;4-Azido-benzoic acid hydrazide;SCHEMBL14060112;DTXSID70431029;4-azidobenzohydrazide, AldrichCPR;AKOS006220444;A1-16722

Chemical Property of Benzoic acid, 4-azido-, hydrazide

Chemical Property:

• Melting Point: 169-170°C
• PSA: 104.87000
• LogP: 1.77586
• Storage Temp.: -20°C, Inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Slightly)
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 177.06505986
• Heavy Atom Count: 13
• Complexity: 227

Purity/Quality:

99% ^*data from raw suppliers

p-Azidobenzoylhydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)NN)N=[N+]=[N-]

Technology Process of Benzoic acid, 4-azido-, hydrazide

There total 3 articles about Benzoic acid, 4-azido-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-azidobenzoic acid (6427-66-3) → p-Azidobenzoyl hydrazide (63296-32-2)

Guidance literature:

Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

2: trifluoroacetic acid / dichloromethane

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ma500384m

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → p-Azidobenzoyl hydrazide (63296-32-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / 1 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

3: trifluoroacetic acid / dichloromethane

With sodium azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ma500384m

Reference yield:

tert-butyl 2-(4-azidobenzoyl)hydrazine carboxylate (1590448-44-4) → p-Azidobenzoyl hydrazide (63296-32-2)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1021/ma500384m

upstream raw materials:

4-azidobenzoic acid

4-amino-benzoic acid

tert-butyl 2-(4-azidobenzoyl)hydrazine carboxylate

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