5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine

Base Information

Chemical Name:5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine
CAS No.:63314-61-4
Molecular Formula:C15H13N3S
Molecular Weight:267.354
Hs Code.:
ChEMBL ID:CHEMBL225063
DSSTox Substance ID:DTXSID90414899
Nikkaji Number:J2.846.348K
Wikidata:Q82223972

Synonyms:63314-61-4;5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine;CHEMBL225063;1,3,4-Thiadiazol-2-amine, N-(4-methylphenyl)-5-phenyl-;DTXSID90414899;BDBM50160592;5-phenyl-N-(p-tolyl)-1,3,4-thiadiazole-2-amine;2-(4-Methylphenylamino)-5-phenyl-1,3,4-thiadiazole

Suppliers and Price of 5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:267.08301860
Heavy Atom Count:19
Complexity:273

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC2=NN=C(S2)C3=CC=CC=C3

Technology Process of 5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine

There total 10 articles about 5-phenyl-N-(p-tolyl)-1,3,4-thiadiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-52-7
benzaldehyde

: 13278-67-6
4-(4-methylphenyl)-3-thiosemicarbazide

: 63314-61-4
N-(4-methylphenyl)-5-phenyl-1,3,4-thiadiazol-2-amine

Guidance literature:: With thiourea; In acetonitrile; at 30 ℃; for 1h;
DOI:10.1002/jhet.367

Reference yield: 80.0%

: 100-52-7
benzaldehyde

: 622-59-3
1-isothiocyanato-4-methylbenzene

: 63314-61-4
N-(4-methylphenyl)-5-phenyl-1,3,4-thiadiazol-2-amine

Guidance literature:: 1-isothiocyanato-4-methylbenzene; With 1-butyl-3-methylimidazolium Tetrafluoroborate; hydrazine;

benzaldehyde; With 1-butyl-3-methylimidazolium Tetrafluoroborate; at 30 - 40 ℃; for 0.416667h; Further stages.;
DOI:10.1002/hc.20432

Reference yield: 78.0%

: 89713-29-1
benzaldehyde 4-p-tolyl-thiosemicarbazone

: 63314-61-4
N-(4-methylphenyl)-5-phenyl-1,3,4-thiadiazol-2-amine

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 20 ℃; for 1h; regioselective reaction;
DOI:10.1016/j.tetlet.2016.01.083