Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)

Base Information

Chemical Name:Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)
CAS No.:63474-24-8
Molecular Formula:C10H19ClMg
Molecular Weight:199.019
Hs Code.:
DSSTox Substance ID:DTXSID40505221

Synonyms:63474-24-8;DTXSID40505221;Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)

Suppliers and Price of Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:198.1025700
Heavy Atom Count:12
Complexity:94.2

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC([CH-]C1)C(C)C.[Mg+2].[Cl-]
Isomeric SMILES:C[C@@H]1CC[C@H]([CH-]C1)C(C)C.[Mg+2].[Cl-]

Technology Process of Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1)

There total 1 articles about Magnesium chloride (2S,5S)-5-methyl-2-(propan-2-yl)cyclohexan-1-ide (1/1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 16052-42-9
(1R,2S,5R)-menthyl chloride

: 63474-24-8
(1R,2S,5R)-(-)menthylmagnesium chloride

Guidance literature:: With ethyl bromide; magnesium; In tetrahydrofuran; 1.) 4 h, 50 degC, 2.) 1 h, 70 deg C;

Reference yield: 94.0%

: 1066-45-1
trimethyltin(IV)chloride

: 63474-24-8
(1R,2S,5R)-(-)menthylmagnesium chloride

: (-)-menthyltrimethyltin

Guidance literature:: In tetrahydrofuran; diethyl ether; exclusion of air and moisture; soln. of Sn-compd. in Et2O added dropwise over a period of 5h at 0°C to a vigorously stirred soln. of Mg-compd. in THF, stirred at room temp. for 48h, treated with water at 0°C, stirred for 1h at room temp.; dried over anhydrous Na2SO4, solvent removed, distn.; elem. anal.;
DOI:10.1016/0022-328X(89)87177-3

Reference yield: 92.0%

: 150689-88-6
dimethylneophyltin bromide

: 63474-24-8
(1R,2S,5R)-(-)menthylmagnesium chloride

: dimethylneophyl(-)-menthyltin

Guidance literature:: In diethyl ether; benzene; N2-atmosphere; dropwise addn. of Grignard reagent (in ether) to Sn-compd. (in C6H6); addn. of 10% HCl, washing of org. layer, drying, evapn.;
DOI:10.1016/0022-328X(95)05323-H