2,2-Dimethylpropyl diphenylphosphinite

Base Information

• Chemical Name: 2,2-Dimethylpropyl diphenylphosphinite
• CAS No.: 63507-05-1
• Molecular Formula: C17H21OP
• Molecular Weight: 272.327
• DSSTox Substance ID: DTXSID60516152
• Wikidata: Q82377436

Synonyms:2,2-Dimethylpropyl diphenylphosphinite;63507-05-1;DTXSID60516152

Chemical Property of 2,2-Dimethylpropyl diphenylphosphinite

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 5
• Exact Mass: 272.133002287
• Heavy Atom Count: 19
• Complexity: 229

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(C)COP(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of 2,2-Dimethylpropyl diphenylphosphinite

There total 1 articles about 2,2-Dimethylpropyl diphenylphosphinite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2,2-dimethyl-propanol-1 (75-84-3) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → 2,2-dimethyl-1-propyl diphenylphosphinite (63507-05-1)

Guidance literature:

With triethylamine; In benzene; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.10.008

Reference yield: 91.0%

2,2-dimethyl-1-propyl diphenylphosphinite (63507-05-1) + methyl iodide (74-88-4) → C18H24OP(1+)*I(1-) (80833-27-8)

Guidance literature:

In diethyl ether; for 168h; Ambient temperature;

DOI:10.1039/P29830001363

Reference yield: 78.0%

2,2-dimethyl-1-propyl diphenylphosphinite (63507-05-1) → 2,2-dimethyl-1-propyl diphenylphosphinothioate (72554-09-7)

Guidance literature:

With sulfur; In toluene; at 80 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tet.2009.10.008

upstream raw materials:

2,2-dimethyl-propanol-1

chloro-diphenylphosphine

Downstream raw materials:

C₁₈H₂₄OP⁽¹⁺⁾*Br^(1-)

C₁₈H₂₄OP⁽¹⁺⁾*Cl^(1-)

2-neopentyloxy-2,3-dihydro-2,2-diphenyl-1,3,2-benzoxazaphosph(V)ole

chloro-diphenylphosphine

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