2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-

Base Information

Chemical Name:2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-
CAS No.:63521-95-9
Molecular Formula:C₅H₇ClOS
Molecular Weight:150.629
Hs Code.:

Synonyms:2-tetrahydrothiophenecarboxylic acid chloride;2-Chlorocarbonyltetrahydrothiophene;2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-;

Suppliers and Price of 2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO- 95.00%
5MG
$ 504.08

Total 3 raw suppliers

Chemical Property of 2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-

Chemical Property:

PSA：42.37000
LogP:1.64740

Purity/Quality:

99% ^*data from raw suppliers

2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO- 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO-

There total 4 articles about 2-THIOPHENECARBONYL CHLORIDE,TETRAHYDRO- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 19418-11-2
(+)-Tetrahydrothiophene-2-carboxylic acid

: 63521-95-9
tetrahydrothiophene-2-carbonyl chloride

Guidance literature:: With thionyl chloride; for 6h;
DOI:10.1021/jo9805044

Reference yield: 83.0%

: 147164-53-2,40053-81-4,154001-94-2
tetrahydropyran-2-carboxylic acid chloride

: 63521-95-9
tetrahydrothiophene-2-carbonyl chloride

Guidance literature:

Reference yield:

: 112212-93-8
(3-Chloropropylthio)acetonitrile

: 63521-95-9
tetrahydrothiophene-2-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / aq. NaOH / TEBA / H₂O / 1 h / Ambient temperature

2: 98 percent / aq. HCl

3: 81 percent / SOCl₂

With hydrogenchloride; sodium hydroxide; thionyl chloride; N-benzyl-N,N,N-triethylammonium chloride; In water;
DOI:10.1055/s-1987-33430