2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one

Base Information

Chemical Name:2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one
CAS No.:63566-54-1
Molecular Formula:C14H9NOS
Molecular Weight:239.298
Hs Code.:
DSSTox Substance ID:DTXSID50493266
Nikkaji Number:J1.620.571K
Wikidata:Q82339821

Synonyms:63566-54-1;N-phenylthiophthalimide;N-phenylthio-phthalimide;SCHEMBL6926171;2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one;DTXSID50493266;RCHBKQDIZMPNEQ-UHFFFAOYSA-N

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:239.04048508
Heavy Atom Count:17
Complexity:335

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C(=O)C3=CC=CC=C3C2=S

Technology Process of 2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one

There total 6 articles about 2-Phenyl-3-sulfanylidene-2,3-dihydro-1H-isoindol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 93-98-1,5705-51-1
N-phenyl benzoyl amide

: 103-72-0
phenyl isothiocyanate

: 63566-54-1
2-phenyl-3-thioxo-2,3-dihydro-1H-isoindol-1-one

Guidance literature:: N-phenyl benzoyl amide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;

phenyl isothiocyanate; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h;
DOI:10.3987/COM-17-13756

Reference yield:

: 520-03-6
N-phenylphthalimide

: 63539-64-0
2-phenyl-1H-isoindole-1,3(2H)-dithione

: 63566-54-1
2-phenyl-3-thioxo-2,3-dihydro-1H-isoindol-1-one

Guidance literature:: With Lawessons reagent; In toluene; for 1h; Heating;
DOI:10.1515/znb-2001-1012

Reference yield:

: 62-53-3
aniline

: 63566-54-1
2-phenyl-3-thioxo-2,3-dihydro-1H-isoindol-1-one

Guidance literature:: Multi-step reaction with 2 steps

2: xylene; aniline; phosphorus pentasulfide

With diphosphorus pentasulfide; aniline; xylene;