Dibenzo[f,h]quinolin-7-ol

Base Information

• Chemical Name: Dibenzo[f,h]quinolin-7-ol
• CAS No.: 5328-26-7
• Molecular Formula: C17H11NO
• Molecular Weight: 245.2753
• Mol file: 5328-26-7.mol

Synonyms:

Chemical Property of Dibenzo[f,h]quinolin-7-ol

Chemical Property:

• Vapor Pressure: 3.67E-11mmHg at 25°C
• Boiling Point: 513.4°C at 760 mmHg
• Flash Point: 264.3°C
• Density: 1.337g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dibenzo[f,h]quinolin-7-ol

There total 2 articles about Dibenzo[f,h]quinolin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-Amino-[3]phenanthrol (85337-42-4) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → dibenzo[f,h]quinolin-7-ol (5328-26-7)

Guidance literature:

With sulfuric acid; iron(II) sulfate; nitrobenzene; at 145 ℃;

DOI:10.1021/jo01209a013

Reference yield:

3-hydroxy-9-nitrophenanthrene (7402-91-7) → dibenzo[f,h]quinolin-7-ol (5328-26-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH-solution; sodium dithionite

2: iron (II)-sulfate; nitrobenzene; sulfuric acid / 145 °C

With sodium hydroxide; sodium dithionite; sulfuric acid; iron(II) sulfate; nitrobenzene;

DOI:10.1021/jo01209a013

upstream raw materials:

9-Amino-[3]phenanthrol

glycerol

3-hydroxy-9-nitrophenanthrene