benzyl 2-(3,4-dimethoxyphenyl)ethylcarbamate

Base Information

Chemical Name:benzyl 2-(3,4-dimethoxyphenyl)ethylcarbamate
CAS No.:63914-27-2
Molecular Formula:C18H21NO4
Molecular Weight:315.369
Hs Code.:
Mol file:63914-27-2.mol

Synonyms:benzyl 3,4-dimethoxyphenethylcarbamate;benzyl 2-(3',4'-dimethoxyphenyl)-ethylaminocarboxylate;

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Chemical Property of benzyl 2-(3,4-dimethoxyphenyl)ethylcarbamate

Chemical Property:

PSA：56.79000
LogP:3.56360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of benzyl 2-(3,4-dimethoxyphenyl)ethylcarbamate

There total 3 articles about benzyl 2-(3,4-dimethoxyphenyl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-iodo-3,4-dimethoxybenzene: 5460-32-2
1-iodo-3,4-dimethoxybenzene

: [2-(9-bora-bicyclo[3.3.1]non-9-yl)-ethyl]-carbamic acid benzyl ester

: 63914-27-2
[2-(3,4-dimethoxy-phenyl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: With sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/jo991064z

Reference yield: 69.0%

: 3459-92-5
DBC

: 124-38-9,18923-20-1
carbon dioxide

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 63914-27-2
[2-(3,4-dimethoxy-phenyl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: at 130 ℃; for 24h; under 90007.2 - 97507.8 Torr;
DOI:10.1039/b508151c

Reference yield:

: 84713-20-2
benzyl N-vinylcarbamate

: 63914-27-2
[2-(3,4-dimethoxy-phenyl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 4 h / -10 - 20 °C

2: 91 percent / aq. NaOH; PdCl₂(dppf)*CH₂Cl₂ / tetrahydrofuran / 1 h / 20 °C

With sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1: Addition / 2: Suzuki coupling;
DOI:10.1021/jo991064z