4-Phenylthiopicolinic acid hydrazide

Base Information

Chemical Name:4-Phenylthiopicolinic acid hydrazide
CAS No.:64064-57-9
Molecular Formula:C12H11N3OS
Molecular Weight:245.305
Hs Code.:
DSSTox Substance ID:DTXSID401229451

Synonyms:64064-57-9;4-phenylthiopicolinic acid hydrazide;SCHEMBL11484939;ZXHIXCFNYQJPDO-UHFFFAOYSA-N;DTXSID401229451;FT-0764254;4-(Phenylthio)-2-pyridinecarboxylic acid hydrazide

Suppliers and Price of 4-Phenylthiopicolinic acid hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 4-Phenylthiopicolinic acid hydrazide

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:245.06228316
Heavy Atom Count:17
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC2=CC(=NC=C2)C(=O)NN

Technology Process of 4-Phenylthiopicolinic acid hydrazide

There total 4 articles about 4-Phenylthiopicolinic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930-69-8
sodium thiophenolate

: 64064-56-8
ethyl 4-chloropyridine-2-carboxylate

: 64064-57-9
4-(phenylthio)-2-picoynoylhydrazide

Guidance literature:: With hydrazine; In hydrogenchloride; methanol;

Reference yield:

: 4-Phenylsulfanyl-pyridine-2-carboxylic acid ethyl ester

: 64064-57-9
4-(phenylthio)-2-picoynoylhydrazide

Guidance literature:: With hydrazine; In methanol; for 1.5h; Yield given; Heating;
DOI:10.1021/jm00144a022

Reference yield:

: 64064-56-8
ethyl 4-chloropyridine-2-carboxylate

: 64064-57-9
4-(phenylthio)-2-picoynoylhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: NaOCH₃ / methanol / 2 h / Heating

2: N₂H₄ / methanol / 1.5 h / Heating

With sodium methylate; hydrazine; In methanol;
DOI:10.1021/jm00144a022