Dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Base Information

Chemical Name:Dibenzo[b,d]thiophen-2-yl(phenyl)methanone
CAS No.:6407-30-3
Molecular Formula:C19H12OS
Molecular Weight:288.37
Hs Code.:
DSSTox Substance ID:DTXSID30496937
Nikkaji Number:J957.791B
Wikidata:Q82346138

Synonyms:Dibenzo[b,d]thiophen-2-yl(phenyl)methanone;6407-30-3;SCHEMBL1576859;DTXSID30496937;WAOFLIDKSDENPS-UHFFFAOYSA-N;(Dibenzo[b,d]thiophen-2-yl)(phenyl)methanone

Suppliers and Price of Dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:288.06088618
Heavy Atom Count:21
Complexity:387

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C2=CC3=C(C=C2)SC4=CC=CC=C43

Technology Process of Dibenzo[b,d]thiophen-2-yl(phenyl)methanone

There total 9 articles about Dibenzo[b,d]thiophen-2-yl(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 132-65-0
dibenzothiophene

: 98-88-4
benzoyl chloride

: 6407-30-3
dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Guidance literature:: aluminum (III) chloride; In 1,2-dichloro-ethane; at 25 ℃; for 2h;

Reference yield: 93.0%

: (2',6-bis(methylthio)-[1,1'-biphenyl]-3-yl)(phenyl)methanone

: 6407-30-3
dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Guidance literature:: With sodium thiomethoxide; In N,N-dimethyl-formamide; at 160 ℃; for 4h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0037-1611974

Reference yield:

: 3-bromo-4-(methylthio)benzonitrile

: 6407-30-3
dibenzo[b,d]thiophen-2-yl(phenyl)methanone

Guidance literature:: Multi-step reaction with 6 steps

1: sodium carbonate / water; toluene / Reflux

2: sodium hydroxide / water; ethanol / Reflux

3: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 5 h / 0 - 20 °C

4: triethylamine / dichloromethane / 0 - 20 °C

5: tetrahydrofuran / 0 - 20 °C

6: sodium thiomethoxide / N,N-dimethyl-formamide / 4 h / 160 °C / Inert atmosphere; Sealed tube

With oxalyl dichloride; sodium carbonate; triethylamine; sodium hydroxide; sodium thiomethoxide; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-0037-1611974