[3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-

Base Information

Chemical Name:[3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-
CAS No.:64089-24-3
Molecular Formula:C₁₄H₁₂N₄
Molecular Weight:236.276
Hs Code.:
DSSTox Substance ID:DTXSID30357574
Nikkaji Number:J3.140.904G
ChEMBL ID:CHEMBL421339

Synonyms:64089-24-3;2',6'-DIMETHYL-1',4'-DIHYDRO-[3,4'-BIPYRIDINE]-3',5'-DICARBONITRILE;HMS1784C12;[3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-;CHEMBL421339;SCHEMBL10663996;DTXSID30357574;AKOS022659806;SR-01000027546;SR-01000027546-1;Z56777657;2',6'-DIMETHYL-1',4'-DIHYDRO-(3,4')BIPYRIDINYL-3',5'-DICARBONITRILE

Suppliers and Price of [3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:236.106196400
Heavy Atom Count:18
Complexity:470

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(C(=C(N1)C)C#N)C2=CN=CC=C2)C#N

Technology Process of [3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl-

There total 1 articles about [3,4'-Bipyridine]-3',5'-dicarbonitrile, 1',4'-dihydro-2',6'-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 25907-38-4
ethyl 4-(phenylthio)-acetoacetate

: 763-33-7
(E)-3-aminocrotononitrile

: 64089-24-3
2,6-dimethyl-3,5-dicyano-4-(3-pyridyl)-1,4-dihydropyridine

: 134968-73-3
5'-Cyano-6'-methyl-2'-phenylsulfanylmethyl-1',4'-dihydro-[3,4']bipyridinyl-3'-carboxylic acid ethyl ester

: (3'S,4'R)-5'-Cyano-6'-methyl-2'-[1-phenylsulfanyl-meth-(Z)-ylidene]-1',2',3',4'-tetrahydro-[3,4']bipyridinyl-3'-carboxylic acid ethyl ester

Guidance literature:: In ethanol; for 24h; Yield given; Heating;
DOI:10.1021/jm00111a047

Reference yield:

: 64089-24-3
2,6-dimethyl-3,5-dicyano-4-(3-pyridyl)-1,4-dihydropyridine

: 1885-14-9
phenyl chloroformate

: 106457-66-3
3',5'-Dicyano-2',6'-dimethyl-1',4'-dihydro-6H-[3,4']bipyridinyl-1-carboxylic acid phenyl ester

: 106457-65-2
3',5'-Dicyano-2',6'-dimethyl-1',4'-dihydro-2H-[3,4']bipyridinyl-1-carboxylic acid phenyl ester

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) CH₃OH, -65 deg C, 10 min, 2.) CH₃OH, ether, -65 deg C, 6 h;
DOI:10.1021/jm00387a010