4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol

Base Information

• Chemical Name: 4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol
• CAS No.: 64230-40-6
• Molecular Formula: C11H20O3
• Molecular Weight: 200.278
• DSSTox Substance ID: DTXSID20473757
• Nikkaji Number: J451.362B

Synonyms:4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol;64230-40-6;SCHEMBL1892052;SCHEMBL18472505;DTXSID20473757;CFWFCOFXUZXFDO-UHFFFAOYSA-N;4-(tetrahydro-2H-pyran-2-yloxy)cyclo-hexanol

Chemical Property of 4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 200.14124450
• Heavy Atom Count: 14
• Complexity: 164

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CCOC(C1)OC2CCC(CC2)O

Technology Process of 4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol

There total 4 articles about 4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,4-dihydro-2H-pyran (110-87-2) + 1,4-Cyclohexanediol (556-48-9) → 1,4-Bis--cyclohexan (736-42-5) + 4-(2-Tetrahydropyranyloxy)-1-cyclohexanol (64230-40-6)

Guidance literature:

With Dowex 50W x 2 (50-100 mesh); In toluene; at 30 ℃; for 1.5h;

DOI:10.1039/c39950002491

Reference yield: 93.0%

3,4-dihydro-2H-pyran (110-87-2) + 1,4-Cyclohexanediol (556-48-9) → 4-(2-Tetrahydropyranyloxy)-1-cyclohexanol (64230-40-6)

Guidance literature:

With pyridinium p-toluenesulfonate; In tetrahydrofuran; for 6h; Ambient temperature;

DOI:10.1021/jo00060a057

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) + 1,4-Cyclohexanediol (556-48-9) → tetrahydro-2H-2-pyranol (694-54-2) + 1,4-Bis--cyclohexan (736-42-5) + 4-(2-Tetrahydropyranyloxy)-1-cyclohexanol (64230-40-6)

Guidance literature:

With Dowex 50W x 2; In toluene; at 30 ℃; for 1.5h;

DOI:10.1021/jo980659b

upstream raw materials:

3,4-dihydro-2H-pyran

1,4-Cyclohexanediol

Downstream raw materials:

4-(tetrahydro-2H-pyran-2-yloxy)cyclohexanone

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