n-Phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine

Base Information

• Chemical Name: n-Phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine
• CAS No.: 4523-36-8
• Molecular Formula: C22H17N3
• Molecular Weight: 323.397
• NSC Number: 138160
• DSSTox Substance ID: DTXSID00300658

Synonyms:4523-36-8;n-phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine;NSC138160;DTXSID00300658;NSC-138160

Chemical Property of n-Phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine

Chemical Property:

• Vapor Pressure: 1.03E-10mmHg at 25°C
• Boiling Point: 514.9°Cat760mmHg
• Flash Point: 265.2°C
• Density: 1.12g/cm³
• XLogP3: 6.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 323.142247555
• Heavy Atom Count: 25
• Complexity: 423

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NC2=C(C3=CC=CC=C3C=C2)N=NC4=CC=CC=C4

Technology Process of n-Phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine

There total 9 articles about n-Phenyl-1-[(e)-phenyldiazenyl]naphthalen-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2]naphthyl-nitroso-phenyl-amine (5488-73-3) + acetic acid (64-19-7,77671-22-8) + aniline (62-53-3) → N-Phenyl-2-naphthylamine (135-88-6,84420-28-0) + N-phenyl-1-(phenyldiazen-yl)naphthalen-2-amine (4523-36-8)

Guidance literature:

Reference yield:

N-Phenyl-2-naphthylamine (135-88-6,84420-28-0) + aniline (62-53-3) → N-phenyl-1-(phenyldiazen-yl)naphthalen-2-amine (4523-36-8)

Guidance literature:

With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.)diazotized 2.)EtOH, 20 deg C, 4 h;

Reference yield:

benzenediazonium (2684-02-8) → N-phenyl-1-(phenyldiazen-yl)naphthalen-2-amine (4523-36-8)

Guidance literature:

With ethanol;

upstream raw materials:

benzenediazonium

N-Phenyl-2-naphthylamine

[2]naphthyl-nitroso-phenyl-amine

acetic acid

Downstream raw materials:

1-Amino-2-anilino-naphthalin

aniline

2,3-diphenyl-naphtho[1,2-d][1,2,3]triazolium; chloride

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