Technology Process of 4,4-Dimethyl-2-phenyl-1,3,2lambda~5~,4-dioxaphosphastannetan-2-one
There total 3 articles about 4,4-Dimethyl-2-phenyl-1,3,2lambda~5~,4-dioxaphosphastannetan-2-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
solid;
Sn-complex was heated under vac. at 130°C for several h; elem. anal.;
- Guidance literature:
-
In
methanol; water;
soln. of Sn-complex in MeOH was added to soln. of ligand in H2O at roomtemp.; filtered, washed with EtOH, dried under vac. at 20°C for 10 h;
- Guidance literature:
-
In
methanol; water;
soln. of Sn-complex in MeOH was added to soln. of ligand in H2O at roomtemp.; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;