4-Bromo-N-morpholinobenzenesulfonamide

Base Information

Chemical Name:4-Bromo-N-morpholinobenzenesulfonamide
CAS No.:64268-87-7
Molecular Formula:C10H13BrN2O3S
Molecular Weight:321.195
Hs Code.:
DSSTox Substance ID:DTXSID201333040
Nikkaji Number:J3.117.927K
ChEMBL ID:CHEMBL1725360

Synonyms:4-Bromo-N-morpholinobenzenesulfonamide;64268-87-7;4-bromo-N-morpholin-4-ylbenzenesulfonamide;MLS001125852;CHEMBL1725360;DTXSID201333040;HMS1590L13;HMS2975I16;STK442075;AKOS003275150;NCGC00229737-01;SMR000665433;CS-0366787;4-bromo-N-(morpholin-4-yl)benzenesulfonamide;4-bromo-N-(morpholin-4-yl)benzene-1-sulfonamide;A914953;BRD-K51064863-001-06-2

Suppliers and Price of 4-Bromo-N-morpholinobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Bromo-N-morpholinobenzenesulfonamide

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:319.98303
Heavy Atom Count:17
Complexity:330

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1NS(=O)(=O)C2=CC=C(C=C2)Br

Technology Process of 4-Bromo-N-morpholinobenzenesulfonamide

There total 5 articles about 4-Bromo-N-morpholinobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 4319-49-7
1-aminomorpholine

: 673-40-5
4-bromobenzenediazonium tetrafluoroborate

: 64268-87-7
4-bromo-N-morpholinobenzenesulfonamide

Guidance literature:: With 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; In acetonitrile; at 25 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1002/anie.201309851

Reference yield: 84.0%

: 4319-49-7
1-aminomorpholine

: 589-87-7
1,4-bromoiodobenzene

: 64268-87-7
4-bromo-N-morpholinobenzenesulfonamide

Guidance literature:: With sulfuric acid; palladium diacetate; caesium carbonate; sodium sulfite; tris[tert-butyl]phosphonium tetrafluoroborate; In 1,4-dioxane; at 80 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.201402212

Reference yield: 38.0%

: 4319-49-7
1-aminomorpholine

: 53601-22-2
4,4'-dibromodiphenyliodonium chloride

: 64268-87-7
4-bromo-N-morpholinobenzenesulfonamide

Guidance literature:: With potassium pyrosulfite; C₃₄H₃₀N₂O₄; trifluoroacetic acid; In dimethyl sulfoxide; acetonitrile; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique; Irradiation;
DOI:10.1002/adsc.201601341