Acetic acid, oxo-, (4-nitrophenyl)methyl ester

Base Information

Chemical Name:Acetic acid, oxo-, (4-nitrophenyl)methyl ester
CAS No.:64370-35-0
Molecular Formula:C9H7NO5
Molecular Weight:209.158
Hs Code.:
DSSTox Substance ID:DTXSID10502005

Synonyms:(4-nitrophenyl)methyl 2-oxoacetate;64370-35-0;p-nitrobenzyl glyoxylate;Acetic acid, oxo-, (4-nitrophenyl)methyl ester;p-nitrobenzyl glyoxalate;SCHEMBL9185772;(4-Nitrophenyl)methyl oxoacetate;DTXSID10502005;HVRMNEPIBIGCNZ-UHFFFAOYSA-N

Suppliers and Price of Acetic acid, oxo-, (4-nitrophenyl)methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Acetic acid, oxo-, (4-nitrophenyl)methyl ester

Chemical Property:

Boiling Point:379.2±44.0 °C(Predicted)
PSA：89.19000
Density:1.381±0.06 g/cm3(Predicted)
LogP:1.36010
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:209.03242232
Heavy Atom Count:15
Complexity:252

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1COC(=O)C=O)[N+](=O)[O-]

Technology Process of Acetic acid, oxo-, (4-nitrophenyl)methyl ester

There total 4 articles about Acetic acid, oxo-, (4-nitrophenyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64406-67-3
di-p-nitrobenzyl tartrate

: 64370-35-0
p-nitrobenzyl glyoxylate

Guidance literature:: With lead(IV) acetate;

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 64370-35-0
p-nitrobenzyl glyoxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N / dimethylformamide / 0.5 h / 0 °C

1.2: 79 percent / dimethylformamide / 0 - 20 °C

2.1: periodic acid / tetrahydrofuran / 1.5 h / 20 °C

2.2: 63 percent / water / tetrahydrofuran / 72 h / 4 °C

3.1: 1.21 g / toluene / Heating

With periodic acid; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1039/b402764g