di-p-nitrobenzyl tartrate

Base Information

• Chemical Name: di-p-nitrobenzyl tartrate
• CAS No.: 64406-67-3
• Molecular Formula: C₁₈H₁₆N₂O₁₀
• Molecular Weight: 420.332
• Mol file: 64406-67-3.mol

Synonyms:di-p-nitrobenzyl tartrate

Chemical Property of di-p-nitrobenzyl tartrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of di-p-nitrobenzyl tartrate

There total 4 articles about di-p-nitrobenzyl tartrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

L-Tartaric acid (87-69-4,138508-61-9) + 1-bromomethyl-4-nitro-benzene (100-11-8) → bis-p-nitrobenzyl tartrate (64406-67-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1080/00397919408011714

Reference yield: 79.0%

tartaric acid (87-69-4,138508-61-9) + 1-bromomethyl-4-nitro-benzene (100-11-8) → di-p-nitrobenzyl tartrate (64406-67-3)

Guidance literature:

tartaric acid; With triethylamine; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

1-bromomethyl-4-nitro-benzene; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1039/b402764g

Reference yield:

1-bromomethyl-4-nitro-benzene (100-11-8) → bis-p-nitrobenzyl tartrate (64406-67-3)

Guidance literature:

With ethanol;

DOI:10.1039/jr9330000760

upstream raw materials:

L-Tartaric acid

1-bromomethyl-4-nitro-benzene

tartaric acid

Downstream raw materials:

p-nitrobenzyl glyoxylate monohydrate

p-nitrobenzyl glyoxylate oxime

p-nitrobenzyl glyoxylate

acetic acid, (dimethoxyphosphinyl)hydroxy-(4-nitrophenyl)methyl ester