Tridec-10-en-1-ol

Base Information

• Chemical Name: Tridec-10-en-1-ol
• CAS No.: 64437-32-7
• Molecular Formula: C13H26O
• Molecular Weight: 198.34500
• Hs Code.: 2905290000
• DSSTox Substance ID: DTXSID40699538
• Mol file: 64437-32-7.mol

Synonyms:tridec-10-en-1-ol;64437-32-7;DTXSID40699538

Chemical Property of Tridec-10-en-1-ol

Chemical Property:

• PSA: 20.23000
• LogP: 4.06570
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 10
• Exact Mass: 198.198365449
• Heavy Atom Count: 14
• Complexity: 118

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCC=CCCCCCCCCCO

Technology Process of Tridec-10-en-1-ol

There total 3 articles about Tridec-10-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-10-decanol (53463-68-6) → (E)-10-tridecen-1-ol (64437-32-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / acetonitrile

2: DMSO, NaH / tetrahydrofuran / 0.5 h

With sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; acetonitrile;

DOI:10.1271/bbb1961.44.257

Reference yield:

10-(Triphenyl-λ5-phosphanylidene)-decan-1-ol (83375-78-4) + propionaldehyde (123-38-6) → (E)-10-tridecen-1-ol (64437-32-7) + (Z)-10-tridecen-1-ol (64437-31-6)

Guidance literature:

In tetrahydrofuran; at -78 - 0 ℃; for 0.5h; Yield given. Yields of byproduct given;

Reference yield:

(10-Hydroxydecyl)-triohenylphosphonium-bromid (64417-10-3) + propionaldehyde (123-38-6) → (E)-10-tridecen-1-ol (64437-32-7) + (Z)-10-tridecen-1-ol (64437-31-6)

Guidance literature:

With sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1271/bbb1961.44.257

upstream raw materials:

10-(Triphenyl-λ⁵-phosphanylidene)-decan-1-ol

propionaldehyde

(10-Hydroxydecyl)-triohenylphosphonium-bromid

1-bromo-10-decanol