p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)-

Base Information

• Chemical Name: p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)-
• CAS No.: 5185-71-7
• Molecular Formula: C₁₀H₁₄AsCl₂NO₃
• Molecular Weight: 342.054
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID20199804
• Nikkaji Number: J33.865F
• Wikidata: Q83072789
• Mol file: 5185-71-7.mol

Synonyms:5185-71-7;BRN 2852551;p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)-;N,N-Bis(2-chloroethyl)-p-arsanilic acid;C10H14AsCl2NO3;DTXSID20199804;C10-H14-As-Cl2-N-O3;Arsanilic acid, N,N-bis(2-chloroethyl)-;LS-21687;4-[N,N-Bis(2-chloroethyl)amino]phenylarsonic acid

Chemical Property of p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)-

Chemical Property:

• Vapor Pressure: 3.09E-13mmHg at 25°C
• Boiling Point: 556.9°Cat760mmHg
• Flash Point: 290.6°C
• PSA: 60.77000
• Density: g/cm³
• LogP: 0.53160
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 340.956668
• Heavy Atom Count: 17
• Complexity: 260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=CC=C1N(CCCl)CCCl)[As](=O)(O)O

Technology Process of p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)-

There total 2 articles about p-ARSANILIC ACID, N,N-BIS(2-CHLOROETHYL)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-arsenoso-N,N-bis-(2-chloro-ethyl)-aniline cyclooligomers (4164-07-2) → N,N-Bis-(2-chloroethyl)-p-arsanilic Acid (5185-71-7)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide;

DOI:10.1021/jm00320a016

Reference yield:

N,N-bis(2-chloroethyl)benzene-1,4-diamine hydrochloride (945-68-6) → N,N-Bis-(2-chloroethyl)-p-arsanilic Acid (5185-71-7)

Guidance literature:

Multistep reaction; (i) NaNO₂, aq. HCl, (ii) aq. Na₃AsO₃, CuSO₄*5H₂O;

DOI:10.1021/jm00320a016

Reference yield:

N,N-Bis-(2-chloroethyl)-p-arsanilic Acid (5185-71-7) → 4--arsenobenzen (4421-46-9)

Guidance literature:

With hydrogenchloride; potassium iodide; tin(ll) chloride; In methanol;

DOI:10.1021/jm00320a016

upstream raw materials:

4-arsenoso-N,N-bis-(2-chloro-ethyl)-aniline cyclooligomers

N,N-bis(2-chloroethyl)benzene-1,4-diamine hydrochloride

Downstream raw materials:

4-arsenoso-N,N-bis-(2-chloro-ethyl)-aniline cyclooligomers

4--arsenobenzen

N,N-bis-(2-chloro-ethyl)-4-[1,3,2]dithiarsolan-2-yl-aniline