Benzoyl chloride, 6-bromo-2,3-dimethoxy-

Base Information

Chemical Name:Benzoyl chloride, 6-bromo-2,3-dimethoxy-
CAS No.:64482-27-5
Molecular Formula:C9H8BrClO3
Molecular Weight:279.518
Hs Code.:
DSSTox Substance ID:DTXSID40473254
Nikkaji Number:J1.278.362K
Wikidata:Q82302548

Synonyms:Benzoyl chloride, 6-bromo-2,3-dimethoxy-;64482-27-5;SCHEMBL422456;DTXSID40473254;2-bromo-5,6-dimethoxybenzoyl chloride

Suppliers and Price of Benzoyl chloride, 6-bromo-2,3-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoyl chloride, 6-bromo-2,3-dimethoxy-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:277.93453
Heavy Atom Count:14
Complexity:212

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)Br)C(=O)Cl)OC

Technology Process of Benzoyl chloride, 6-bromo-2,3-dimethoxy-

There total 6 articles about Benzoyl chloride, 6-bromo-2,3-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.7%

: 60555-93-3
6-bromo-2,3-dimethoxybenzoic acid

: 64482-27-5
2-bromo-5,6-dimethoxybenzoyl chloride

Guidance literature:: With thionyl chloride; In benzene; for 1h; Heating;

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 64482-27-5
2-bromo-5,6-dimethoxybenzoyl chloride

Guidance literature:: With sodium hydroxide; thionyl chloride; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; Multistep reaction;
DOI:10.1016/00404-0399(50)1364-N

Reference yield:

: 53811-50-0
6-bromo-2,3-dimethoxybenzaldehyde

: 64482-27-5
2-bromo-5,6-dimethoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / KMnO₄ / acetone; H₂O / 3 h / 50 - 60 °C

2: 90.7 percent / SOCl₂ / benzene / 1 h / Heating

With potassium permanganate; thionyl chloride; In water; acetone; benzene;