2-METHOXY-5-(TRIFLUOROMETHYL)BENZOYL CHLORIDE

Base Information

• Chemical Name: 2-METHOXY-5-(TRIFLUOROMETHYL)BENZOYL CHLORIDE
• CAS No.: 64507-07-9
• Molecular Formula: C9H6ClF3O2
• Molecular Weight: 238.594
• Hs Code.: 2918990090

Synonyms:2-METHOXY-5-(TRIFLUOROMETHYL)NICOTINALDEHYDE;2-METHOXY-5-(TRIFLUOROMETHYL)PYRIDINE-3-CARBOXALDEHYDE;2-Methoxy-5-(trifluoromethyl)-3-pyridinecarboxaldehyde;5-(TRIFLUOROMETHYL)-2-METHOXYPYRIDINE-3-CARBALDEHYDE;

Chemical Property of 2-METHOXY-5-(TRIFLUOROMETHYL)BENZOYL CHLORIDE

Chemical Property:

• PSA: 26.30000
• LogP: 3.09300

Purity/Quality:

95% ^*data from raw suppliers

2-Methoxy-5-(trifluoromethyl)benzoyl chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-METHOXY-5-(TRIFLUOROMETHYL)BENZOYL CHLORIDE

There total 1 articles about 2-METHOXY-5-(TRIFLUOROMETHYL)BENZOYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-5-(trifluoromethyl)-benzoic acid (4864-01-1) → 2-methoxy-5-trifluoromethylbenzoyl chloride (64507-07-9)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1021/jm9803572

Reference yield: 82.0%

(S)-2-((tetrahydrofuran-2-yl)methyl)-2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-amine (1140917-69-6) + 2-methoxy-5-trifluoromethylbenzoyl chloride (64507-07-9) → 2-methoxy-N-{2-[(2R)-tetrahydrofuran-2-ylmethyl]-2,4,5,6-tetrahydrocyclopenta[c]pyrazol-3-yl}-5-(trifluoromethyl)benzamide (1140917-70-9)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 36.3%

3-tert-butyl-1-((tetrahydrofuran-3-yl)methyl)-1H-pyrazol-5-amine hydrogen + 2-methoxy-5-trifluoromethylbenzoyl chloride (64507-07-9) → N-(3-tert-butyl-1-((tetrahydrofuran-3-yl)methyl)-1H-pyrazol-5-yl)-2-methoxy-5-(trifluoromethyl)benzamide (1140918-65-5)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water; at 25 ℃; for 12h;

upstream raw materials:

2-methoxy-5-(trifluoromethyl)-benzoic acid

Downstream raw materials:

β-{4-[2-(2-methoxy-5-trifluoromethylbenzamido)-ethyl]-phenyl}-propionic acid

Ethyl 3-[2-methoxy-5-(trifluoromethyl)phenyl]-3-oxopropanoate

(Z)-tert-butyl 3-((5-tert-butyl-2-(2-methoxy-5-(trifluoromethyl)benzoylimino)thiazol-3(2H)-yl)methyl)azetidine-1-carboxylate

N-[(5Z)-4-butyl-2-(2-fluoro-1,1-dimethylethyl)isothiazol-5(2H)-ylidene]-2-methoxy-5-(trifluoromethyl)benzamide

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