Tridecanal, oxime

Base Information

• Chemical Name: Tridecanal, oxime
• CAS No.: 646-28-6
• Molecular Formula: C13H27NO
• Molecular Weight: 213.363
• Mol file: 646-28-6.mol

Synonyms:

Chemical Property of Tridecanal, oxime

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tridecanal, oxime

There total 1 articles about Tridecanal, oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-dodecene (112-41-4,25067-08-7,62132-67-6) + carbon monoxide (201230-82-2) → dodecane (112-40-3) + tridecanenitrile (629-60-7) + (E)-tridecanal oxime (646-28-6) + C26H50O + (Z)-tridecanal oxime + C14H29NO

Guidance literature:

With acetylacetonatodicarbonylrhodium(l); hydrogen; hydroxylamine; 9,9-dimethyl-2,7-bissulfonato-4,5-bis(diphenylphosphino)xanthene-sodium salt; In water; butan-1-ol; at 100 ℃; for 4h; under 45004.5 Torr; regioselective reaction; Catalytic behavior;

DOI:10.1039/d0gc03141k

Reference yield: 76.0%

tridecanal oxime (646-28-6) → tridecanenitrile (629-60-7)

Guidance literature:

With diethyl cyanophosphonate; triethylamine; In dichloromethane; at 20 ℃; for 20h; Reagent/catalyst; Concentration; Temperature; Inert atmosphere;

DOI:10.5012/bkcs.2012.33.10.3173

Reference yield:

tridecanal oxime (646-28-6) → tridecanal (10486-19-8)

Guidance literature:

Yield given;

DOI:10.1016/S0040-4039(00)84510-4

upstream raw materials:

1-dodecene

carbon monoxide

Downstream raw materials:

tridecanal

tridecanenitrile

Refernces