Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-

Base Information

Chemical Name:Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-
CAS No.:647028-05-5
Molecular Formula:C17H16O3S
Molecular Weight:300.378
Hs Code.:
DSSTox Substance ID:DTXSID30478117
Wikidata:Q82311308

Synonyms:647028-05-5;Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-;DTXSID30478117

Suppliers and Price of Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:300.08201554
Heavy Atom Count:21
Complexity:487

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=C(CC2)S(=O)(=O)C3=CC=CC=C3

Technology Process of Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]-

There total 1 articles about Benzene, 1-methoxy-4-[2-(phenylsulfonyl)-1-cyclobuten-1-yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 105858-77-3
1,2-bis(phenylsulfonyl)-1-cyclobutene

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 647028-05-5
1-phenylsulfonyl-2-p-methoxyphenyl-1-cyclobutene

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1002/chem.200304902

Reference yield: 82.0%

: 591-51-5
phenyllithium

: 647028-05-5
1-phenylsulfonyl-2-p-methoxyphenyl-1-cyclobutene

: 58368-36-8
1-methoxy-4-(2-phenyl-1-cyclobuten-1-yl)benzene

Guidance literature:: In tetrahydrofuran; toluene; at 0 ℃; for 0.5h;
DOI:10.1002/chem.200304902

Reference yield:

: 647028-05-5
1-phenylsulfonyl-2-p-methoxyphenyl-1-cyclobutene

: anti-1-(4-methoxyphenyl)-4-phenyl-1,4-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / tetrahydrofuran; toluene / 0.5 h / 0 °C

2.1: BH₃*THF / tetrahydrofuran / 5.5 h / 0 - 50 °C

2.2: 89 percent / aq. NaOH; H₂O₂ / tetrahydrofuran / 0 °C

With borane-THF; In tetrahydrofuran; toluene;
DOI:10.1002/chem.200304902