delta-Tetradecalactone

Base Information

• Chemical Name: delta-Tetradecalactone
• CAS No.: 92446-06-5
• Molecular Formula: C₁₄H₂₆O₂
• Molecular Weight: 226.359
• Hs Code.: 2932209090
• Mol file: 92446-06-5.mol

Synonyms:Tetradecanolactone;tetrahydro-6-nonyl-2H-pyran-2-one;6-NONYL-3,4,5,6-TETRAHYDRO-2H-2-PYRANONE;5-TETRADECANOLIDE;DELTA-TETRADECALACTONE;DELTA-TETRADECANOLACTONE;6-nonyltetrahydro-2H-pyran-2-one;6-nonyl-tetrahydro-pyran-2-one;

Chemical Property of delta-Tetradecalactone

Chemical Property:

• Refractive Index: n20/D 1.461(lit.)
• Boiling Point: 130-135 °C5 mm Hg(lit.)
• Flash Point: >230 °F
• PSA: 26.30000
• Density: 0.936 g/mL at 20 °C(lit.)
• LogP: 4.22280

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Safety Statements: 23-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of delta-Tetradecalactone

There total 5 articles about delta-Tetradecalactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-nonyl-cyclopentanone (40566-27-6) → tetrahydro-6-nonyl-2H-pyran-2-one (92446-06-5,129263-76-9,141980-54-3,2721-22-4)

Guidance literature:

With MoOBr₃; dihydrogen peroxide; acetic anhydride; acetic acid; at 50 - 70 ℃; for 6h;

Reference yield: 7.9%

5-hydroxytetradecanethioamide → tetrahydro-6-nonyl-2H-pyran-2-one (92446-06-5,129263-76-9,141980-54-3,2721-22-4)

Guidance literature:

With Novozym 435 from Candida antarctica B; In diethyl ether; at 40 ℃; for 48h; Reagent/catalyst; Enzymatic reaction;

DOI:10.1515/hc-2019-0103

Reference yield:

5-acetoxytetradecanamide → tetrahydro-6-nonyl-2H-pyran-2-one (92446-06-5,129263-76-9,141980-54-3,2721-22-4)

Guidance literature:

Multi-step reaction with 3 steps

1: Lawessons reagent / toluene / 0.08 h / 80 °C

2: sodium methylate / methanol / 0.5 h / -15 °C

3: Novozym 435 from Candida antarctica B / diethyl ether / 48 h / 40 °C / Enzymatic reaction

With Lawessons reagent; sodium methylate; Novozym 435 from Candida antarctica B; In methanol; diethyl ether; toluene;

DOI:10.1515/hc-2019-0103

upstream raw materials:

2-nonyl-cyclopentanone

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