Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI)

Base Information

Chemical Name:Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI)
CAS No.:648881-65-6
Molecular Formula:C14H13N3O2
Molecular Weight:255.276
Hs Code.:
Mol file:648881-65-6.mol

Synonyms:Benzamide,N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl];

Suppliers and Price of Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI)

Chemical Property:

PSA：67.48000
LogP:1.51580

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI)

There total 1 articles about Benzamide, N-[1,2-dihydro-2-oxo-1-(2-propenyl)-4-pyrimidinyl]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 591-87-7
Allyl acetate

: 26661-13-2
4-N-benzoylcytosine

: 648881-65-6
N-(1-allyl-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Guidance literature:: 4-N-benzoylcytosine; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 60 ℃; for 45h;

Allyl acetate; With 1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 60 ℃; for 10h;
DOI:10.1021/acs.joc.8b02442

Reference yield: 69.0%

: 648881-65-6
N-(1-allyl-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

: 62853-19-4
(S)-N-(1-(2,3-dihydroxypropyl)-2-oxo-1,2-dihydropyrimidin-4-yl)benzamide

Guidance literature:: With potassium osmate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 - 20 ℃;
DOI:10.1021/acs.joc.8b02442